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Inorganic Chemistry Communications

Inorganic Chemistry Communications

IF: 4.4
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Enhancing the synthetic efficacy of thorium tetrachloride bis(1,2-dimethoxyethane) with added 1,2-dimethoxyethane: Preparation of metallocene thorium dichlorides

Published:1 August 2014 DOI: 10.1016/j.inoche.2014.04.028
Marisa J. Monreal, Robert K. Thomson, Brian L. Scott, Jaqueline L. Kiplinger

Abstract

The synthetic efficacy of thorium tetrachloride bis(dimethoxyethane), ThCl4(DME)2, is improved by adding 1,2-dimethoxyethane (DME) to the reaction mixture. The syntheses of the known metallocene dichlorides (C5Me5)2ThCl2 (1), (1,2,4-tBu3-C5H2)2ThCl2 (2), and (C5Me4Et)2ThCl2 (3) are used to demonstrate this finding. The full characterization and X-ray crystal structure of (C5Me4Et)2ThCl2 (3) is also reported.

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Procduct Name CAS Molecular Formula Supplier Price
1,2-Dimethoxyethane 110-71-4 C4H10O2 545 suppliers $13.00-$1670.00
Di-μ-iododiiodobis[(1,2,3,4,5-η)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl]dicobalt 72339-52-7 C20H32Co2I4 12 suppliers Inquiry
1,2-Dimethoxyethane 143585-58-4 C4H10O2 8 suppliers $130.00-$130.00
MOLYBDENUM TETRACHLORIDE DIMETHOXYETHANE COMPLEX 134535-29-8 C4H10Cl4MoO2 7 suppliers Inquiry
DME Antibody 4 suppliers Inquiry

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