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Organic & Biomolecular Chemistry

Organic & Biomolecular Chemistry

IF: 2.89
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Deoxygenative cross-electrophile coupling of benzyl chloroformates with aryl iodides1

Published:7 May 2019 DOI: 10.1039/c9ob00628a PMID: 30951058
Yingying Pan , Yuxin Gong , Yanhong Song , Weiqi Tong , Hegui Gong

Abstract

This work describes Ni-catalyzed cross-electrophile coupling of benzyl chloroformate derivatives with aryl iodides that generates a wide range of diaryl methane products. The mild reaction conditions merit the C–O bond radical fragmentation of benzyl chloroformates via halide abstraction or a single electron reduction by a Ni catalyst. This work offers a new substrate type for cross-electrophile couplings.

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