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513-38-2

碘代異丁烷(513-38-2)質(zhì)譜(MS)

產(chǎn)品名稱:碘代異丁烷

CAS:513-38-2

分子式:C4H9I

分子量: 184.02

InChI:InChI=1S/C4H9I/c1-4(2)3-5/h4H,3H2,1-2H3

InChIKey: BTUGGGLMQBJCBN-UHFFFAOYSA-N

Smiles:C(I)C(C)C

  • 圖譜
    Mass 

    MS-NW-1595          
1-iodo-2-methylpropane
C4H9I               (Mass of molecular ion:    184)


       Source Temperature: 240 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          15.0       1.2
      27.0       8.6
      29.0      36.8
      38.0       1.4
      39.0      11.8
      40.0       1.6
      41.0      46.8
      42.0       3.6
      43.0       2.9
      55.0       4.4
      56.0       1.4
      57.0     100.0
      58.0       4.5
      97.0       1.2
     127.0       2.4
     184.0      13.3

90 MHz in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C4 H9 I 0.05 ml : 0.5 ml CDCl3
    1-iodo-2-methylpropane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             3.139
      B             1.74
      C             1.02
     
     J(A,B)=5.8HZ. J(B,C)=6.3HZ.
  

         Hz     ppm     Int.


        284.31   3.175    463
    278.50   3.110    521
    167.63   1.872     25
    162.75   1.818     25
    161.56   1.804     37
    160.81   1.796     21
    156.88   1.752     21
    155.69   1.739     50
    154.56   1.726     43
    149.69   1.672     29
    148.69   1.661     52
    142.69   1.594     44
     93.50   1.044   1000
     87.19   0.974    717

in CDCl3

  • 圖譜

CCl4 solution

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liquid film

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REACTION WITH NA AT 77K

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