31729-66-5

1-苯基環(huán)丙基甲醇(31729-66-5)核磁圖(¹³CNMR)

產(chǎn)品名稱(chēng):1-苯基環(huán)丙基甲醇

CAS:31729-66-5

分子式:C10H12O

分子量: 148.2

Mass

MS-IW-0565          
1-phenyl-1-cyclopropanemethanol
C10H12O             (Mass of molecular ion:    148)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      18.0       1.2
      27.0       5.0
      28.0       1.3
      29.0       1.5
      31.0       3.8
      38.0       1.0
      39.0      15.0
      40.0       1.5
      41.0       6.7
      42.0       1.2
      43.0       4.3
      50.0       4.6
      51.0      16.6
      52.0       4.1
      53.0       2.5
      55.0       8.5
      57.0       1.8
      62.0       2.1
      63.0       8.9
      64.0       5.3
      65.0      15.0
      66.0       1.7
      69.0       2.8
      70.0       1.3
      74.0       1.8
      75.0       2.7
      76.0       3.5
      77.0      18.6
      78.0      17.5
      79.0       7.5
      89.0       7.4
      90.0       2.4
      91.0      89.1
      92.0      14.9
      93.0       1.0
     102.0       6.7
     103.0       9.3
     104.0       8.5
     105.0      22.0
     106.0       8.3
     107.0       1.7
     115.0      64.0
     116.0      14.6
     117.0     100.0
     118.0      43.0
     119.0       9.4
     120.0      25.3
     121.0       2.2
     127.0       3.3
     128.0       7.5
     129.0      18.5
     130.0      36.5
     131.0       5.8
     133.0      20.1
     134.0       2.0
     147.0       6.4
     148.0      32.2
     149.0       3.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₂ O	0.039 g : 0.5 ml CDCl₃
1-phenyl-1-cyclopropanemethanol

    Assign.     Shift(ppm)

      A             7.344
      B             7.300
      C             7.211
      D             3.628
      E             1.65
      F     *1      0.863
      G     *1      0.830

     Hz     ppm     Int.

   2941.77   7.361    427
   2940.19   7.357    568
   2938.11   7.352    207
   2935.30   7.345    285
   2934.20   7.342    483
   2933.35   7.340    993
   2932.01   7.337    883
   2930.18   7.332    215
   2924.56   7.318    475
   2923.95   7.317    710
   2922.00   7.312    213
   2920.17   7.307     64
   2918.58   7.303    230
   2917.48   7.301    622
   2916.75   7.299   1000
   2915.16   7.295    396
   2910.64   7.283    243
   2908.94   7.279    414
   2907.10   7.275     95
   2889.40   7.230    235
   2887.82   7.226    447
   2886.23   7.222    244
   2884.28   7.218     38
   2882.93   7.214    184
   2880.62   7.208    411
   2878.42   7.203    148
   2875.00   7.194    118
   2873.54   7.191    201
   2872.07   7.187    109
   1450.20   3.629    905
    659.79   1.651    249
    354.86   0.888     61
    352.66   0.883    172
    350.59   0.878     34
    345.95   0.866    741
    345.09   0.864    759
    343.02   0.859    578
    342.04   0.856    662
    334.47   0.837    716
    333.50   0.835    709
    332.28   0.832    688
    331.67   0.830    771
    330.81   0.828    773
    330.32   0.827    743
    323.97   0.811    194
    321.90   0.806     67

in CDCl3