2415-80-7

(2,2-二氯環(huán)丙基)苯(2415-80-7)質(zhì)譜(MS)

產(chǎn)品名稱:(2,2-二氯環(huán)丙基)苯

CAS:2415-80-7

分子式:C9H8Cl2

分子量: 187.07

InChI:InChI=1S/C9H8Cl2/c10-9(11)6-8(9)7-4-2-1-3-5-7/h1-5,8H,6H2

InChIKey: WLWFQGXZIDYWQF-UHFFFAOYSA-N

Smiles:C1(C2CC2(Cl)Cl)=CC=CC=C1

Mass

MS-IW-1263          
(2,2-dichlorocyclopropyl)benzene
C9H8Cl2             (Mass of molecular ion:    186)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      38.0       1.2
      39.0       5.0
      50.0       3.7
      51.0       6.4
      52.0       1.2
      57.0       6.9
      57.5       6.7
      58.0       2.2
      61.0       1.2
      62.0       3.0
      63.0       7.8
      64.0       1.5
      65.0       3.5
      73.0       1.8
      74.0       2.9
      74.5       1.1
      75.0       5.0
      75.5       1.0
      76.0       1.9
      77.0       4.0
      78.0       3.0
      86.0       1.1
      87.0       1.6
      88.0       1.0
      89.0       9.0
      90.0       2.5
      91.0       4.0
     102.0       1.3
     103.0       2.7
     104.0       2.1
     113.0       1.4
     114.0       2.6
     115.0     100.0
     116.0      21.7
     117.0       1.6
     125.0       2.1
     149.0       5.3
     150.0       3.1
     151.0      64.5
     152.0       7.2
     153.0      20.4
     154.0       2.0
     186.0      18.4
     187.0       2.1
     188.0      11.8
     189.0       1.2
     190.0       1.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₈ Cl₂	0.05 ml : 0.5 ml CDCl₃
(2,2-dichlorocyclopropyl)benzene

    Assign.     Shift(ppm)

      A             7.314
      B             7.273
      C             7.214
      D             2.868
      E             1.910
      F             1.810

     Hz     ppm     Int.

   2933.84   7.342    194
   2932.13   7.337    335
   2930.42   7.333    159
   2927.37   7.325    218
   2925.42   7.320    886
   2923.58   7.316    576
   2919.31   7.305    406
   2917.85   7.302   1000
   2912.84   7.289    257
   2911.25   7.285    542
   2909.67   7.281    385
   2906.86   7.274    162
   2904.17   7.267    553
   2900.76   7.259    120
   2898.32   7.253     99
   2896.85   7.249    143
   2895.51   7.246     75
   2887.45   7.225    789
   2885.86   7.221    970
   2883.67   7.216    291
   2879.27   7.205    702
   2878.66   7.203    713
   1156.25   2.894    331
   1147.71   2.872    368
   1145.63   2.867    385
   1137.08   2.846    369
    772.95   1.935    516
    765.50   1.916    707
    762.33   1.908    505
    754.88   1.889    681
    730.83   1.829    652
    723.14   1.810    626
    722.41   1.808    707
    714.97   1.789    464

in CDCl3