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20600-44-6

5-氯-2-苯駢噻唑酮(20600-44-6)紅外圖譜(IR1)

產(chǎn)品名稱:5-氯-2-苯駢噻唑酮

CAS:20600-44-6

分子式:C7H4ClNOS

分子量: 185.63

InChI:InChI=1S/C7H4ClNOS/c8-4-1-2-6-5(3-4)9-7(10)11-6/h1-3H,(H,9,10)

InChIKey: NOVHYVKPKWACML-UHFFFAOYSA-N

Smiles:S1C2=CC=C(Cl)C=C2NC1=O

  • 圖譜
    Mass

    MS-NW-9394          
    5-chloro-2(3H)-benzothiazolone
    C7H4ClNOS           (Mass of molecular ion:    185)
    

       Source Temperature: 200 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       4.9
          28.0       1.8
          36.0       1.0
          37.0       2.3
          38.0       2.7
          39.0       1.2
          44.0       1.3
          45.0       8.8
          47.0       1.7
          49.0       1.2
          50.0       3.3
          51.0       3.3
          52.0       2.4
          57.0       1.3
          60.0       1.0
          60.5       3.9
          61.0       6.1
          62.0       3.9
          63.0       6.1
          64.0       1.2
          69.0       8.6
          70.0       2.5
          71.0       1.4
          73.0       1.7
          74.0       1.0
          75.0       1.3
          76.0       2.8
          78.0       2.1
          78.5       5.0
          79.0       1.3
          79.5       1.8
          81.0       1.4
          82.0       1.1
          92.5       2.4
          93.0       3.8
          94.0       2.5
          95.0      19.6
          96.0       1.6
          97.0       1.5
         106.0       1.5
         107.0       2.3
         112.0       1.0
         120.0       1.3
         121.0       4.3
         122.0      32.5
         123.0       2.7
         124.0       2.4
         129.0       1.0
         130.0      30.8
         131.0       2.4
         132.0      11.3
         142.0       1.0
         149.0       1.3
         150.0       2.3
         156.0       1.6
         157.0      45.2
         158.0       4.1
         159.0      16.7
         160.0       1.3
         185.0     100.0
         186.0       9.4
         187.0      36.8
         188.0       3.3
         189.0       1.6
    

400 MHz in DMSO-d6

  • 圖譜

    1H NMR 399.65 MHz
    C7 H4 Cl N O S 0.031 g : 0.5 ml DMSO-d6
    5-chloro-2(3H)-benzothiazolone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.07 B 7.606 C 7.188 D 7.137

         Hz     ppm     Int.
    

       4824.24  12.072    141
       3053.20   7.640     22
       3044.23   7.618    809
       3039.83   7.607     93
       3035.80   7.597    884
       3028.11   7.577     24
       2886.89   7.224     23
       2878.10   7.202    561
       2875.90   7.197    630
       2869.67   7.181    500
       2867.65   7.176    583
       2863.26   7.165     69
       2861.79   7.161     60
       2861.06   7.159     59
       2853.37   7.140   1000
       2851.35   7.135    878
       2841.10   7.109     25
       2840.55   7.108     24
       2838.71   7.103     22
    

in DMSO-d6

  • 圖譜

KBr disc

  • 圖譜

nujol mull

  • 圖譜

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