1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE

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1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE manufacturers

1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE Basic information

Product Name:	1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE
Synonyms:	4-Methoxy-2-(trimethylsiloxy)-1,3-butadiene;4-Methoxy-2-(trimethylsilyloxy)-1,3-butadiene;Trimethyl[(1-methylene-3-methoxy-2-propenyl)oxy]silane;1-Methoxy-3-(trimethylsilyloxy)-1,3-butadiene,90%;DANISHEFSKY'S DIENE;methyl 3-trimethylsilyloxybuta-1,3-dien-1-yl ether;1-Me-3-(trimEtsilyloxy)-1,3-butadiene;([(2E)-3-Methoxy-1-methylene-2-propenyl]oxy)(trimethyl)silane
CAS:	59414-23-2
MF:	C8H16O2Si
MW:	172.3
EINECS:	261-753-0
Product Categories:	Monoalkoxysilanes;Si (Classes of Silicon Compounds);Silicon Compounds (for Synthesis);Si-O Compounds;Synthetic Organic Chemistry;Vinylsilanes, Allylsilanes
Mol File:	59414-23-2.mol

1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE Chemical Properties

Boiling point	68-69 °C14 mm Hg(lit.)
density	0.885 g/mL at 25 °C(lit.)
refractive index	n20/D 1.454(lit.)
Fp	113 °F
storage temp.	2-8°C
solubility	insol H2O; sol most organic solvents
form	Liquid
color	Clear light yellow to brown
Merck	14,6001
CAS DataBase Reference	59414-23-2(CAS DataBase Reference)
EPA Substance Registry System	Silane, [(3-methoxy-1-methylene-2-propenyl)oxy]trimethyl- (59414-23-2)

Safety Information

MSDS Information

1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE Usage And Synthesis

Chemical Properties	CLEAR LIGHT YELLOW TO BROWN LIQUID
Uses	1-Methoxy-3-trimethylsilyloxy-1,3-butadiene is used as a highly reactive diene for Diels-Alder reactions and hetero-Diels-Alder reactions.
Preparation	1-Methoxy-3-trimethylsilyloxy-1,3-butadiene was originally prepared from 4-Methoxy-3-buten-2-one with Chlorotrimethylsilane-Triethylamine-Zinc Chloride in benzene as shown below (68% yield, eq 1). At the present time, the most efficient method is to use TMSCl-Lithium Bromide-Et3N in THF (91%).
storage	1-Methoxy-3-trimethylsilyloxy-1,3-butadiene can be kept in a stoppered container without appreciable decomposition, but it is extremely moisture sensitive.

1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE Preparation Products And Raw materials

Preparation Products

Tag:1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE(59414-23-2) Related Product Information

POLYBUTADIENE BIS(TRIMETHYLSILYL) SULFIDE 2-(Trimethylsiloxy)-1,3-butadiene 1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE (1Z)-1-(Benzyloxy)-3-methoxy-1-(trimethylsiloxy)-1,3-butadiene