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| | (S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Basic information |
| Product Name: | (S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE | | Synonyms: | ALPHA,N,N-TRIMETHYLBENZYLAMINE;(1S)-N,N-Dimethyl-1-phenylethanamine;(S)-N,N,α-Trimethylbenzenemethanamine;(αS)-N,N,α-Trimethylbenzenemethanamine;[(S)-α-Methylbenzyl]dimethylamine;[S,(-)]-N,N,α-Trimethylbenzenemethanamine;[S,(-)]-N,N-Dimethyl-1-phenylethanamine;(S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE, 9 7% | | CAS: | 17279-31-1 | | MF: | C10H15N | | MW: | 149.23 | | EINECS: | 241-310-8 | | Product Categories: | | | Mol File: | 17279-31-1.mol |  |
| | (S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Chemical Properties |
| Melting point | 143°C (estimate) | | Boiling point | 81 °C/16 mmHg (lit.) | | density | 0.899 g/mL at 25 °C (lit.) | | refractive index | n20/D 1.503 | | Fp | 148 °F | | storage temp. | 2-8°C | | pka | 8.88±0.50(Predicted) | | form | clear liquid | | color | Colorless to Light yellow to Light orange | | optical activity | [α]20/D 49.2°, c = 1 in methanol | | BRN | 3196218 | | CAS DataBase Reference | 17279-31-1(CAS DataBase Reference) |
| Hazard Codes | Xn | | Risk Statements | 22-36 | | Safety Statements | 26 | | RIDADR | 2810 | | WGK Germany | 2 | | F | 8-10-23 | | HS Code | 2921490090 |
| | (S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Usage And Synthesis |
| Chemical Properties | clear colorless to yellow liquid | | Purification Methods | The amine is mixed with aqueous 10N NaOH and extracted with toluene. The extract is washed with saturated aqueous NaCl, dried over K2CO3, and transferred to fresh K2CO3 until the solution is clear, and is filtered. The filtrate is distilled. If a short column packed with glass helices is used, the yield is reduced but a purer product is obtained. [Ingersoll Org Synth 25 89 1945, Snyder & Brewster J Am Chem Soc 71 291 4165 1949, Cope et al. J Am Chem Soc 71 3931 1949.] The (-)-picrate has m 140-141o from EtOH). The racemate [1126-71-2] has b 88-89o/16mm, 92-94o/30mm, 194-195o/760mm, d4 0.908. [Beilstein 13 III 2392.] |
| | (S)-(-)-N,N-DIMETHYL-1-PHENETHYLAMINE Preparation Products And Raw materials |
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