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1-[[(9H-???-9-????)???]??]-2,5-??????

1-[[(9H-???-9-????)???]??]-2,5-??????
1-[[(9H-???-9-????)???]??]-2,5-?????? ??? ???
?? ??:
82911-69-1
???:
1-[[(9H-???-9-????)???]??]-2,5-??????
???(??):
1-[[(9H-???-9-????)???]??]-2,5-??????(CASNo.82911-69-1);1-[[(9H-???-9-????)???]??]-2,5-??????
???:
N-(9-Fluorenylmethoxycarbonyloxy)succinimide
???(??):
FMOC-OSU;Fomc-Osu;(9H-Fluoren-9-yl)Methyl (2,5-dioxopyrrolidin-1-yl) carbonate;FMOC N-HYDROXYSUCCINIMIDE ESTER;FMOC-SU;FMOC-ONSU;9-FLUORENYLMETHYL SUCCINIMIDYL CARBONATE;FMOC-Succinimide;9-fluorenylmethyl-n-succinimide carbonate;9-FLUORENYLMETHYL N-SUCCINIMIDYL CARBONATE
CBNumber:
CB9428667
???:
C19H15NO5
??? ??:
337.33
MOL ??:
82911-69-1.mol
MSDS ??:
SDS

1-[[(9H-???-9-????)???]??]-2,5-?????? ??

???
150-153 °C(lit.)
?? ?
150-153°C
??
1.3460 (rough estimate)
???
1.5000 (estimate)
?? ??
2-8°C
???
??? ???? ? ??? ?????? ?????.
??? ??
???? ??
??
?? ?? ?? ??
??
Moisture Sensitive
BRN
3569540
???
??? ???
CAS ??????
82911-69-1(CAS DataBase Reference)
??
  • ?? ? ?? ??
  • ?? ? ???? ?? (GHS)
??? ?? Xi,N,Xn
?? ???? ?? 36/37/38-51/53-43-22
????? 22-24/25-26/37/39-26-61-37-24
????(UN No.) UN 3077 9 / PGIII
WGK ?? 3
F ?????? 10-21
?? ?? ?? Moisture Sensitive
?? ?? 9
HS ?? 29251995
???? ?? 2001-3-1751
????(GHS): GHS hazard pictogramsGHS hazard pictograms
?? ?: Warning
??·?? ??:
?? ??·?? ?? ?? ?? ?? ?? ? ?? ?? P- ??
H302 ??? ??? ?? ?? ?? - ?? ?? 4 ?? GHS hazard pictograms P264, P270, P301+P312, P330, P501
H317 ????? ?? ??? ??? ? ?? ?? ??? ?? ?? 1 ?? GHS hazard pictograms P261, P272, P280, P302+P352,P333+P313, P321, P363, P501
H411 ??? ??? ?? ????? ??? ?? ????? ?? - ?? ?? 2
??????:
P261 ??·?·??·???·??·...·????? ??? ????.
P264 ?? ??? ?? ??? ????.
P264 ?? ??? ?? ??? ????.
P273 ???? ???? ???.
P280 ????/???/???/?????? ?????.
P301+P312 ??? ???? ??? ????(??)? ??? ????.
P302+P352 ??? ??? ??? ?? ????.
NFPA 704
0
2 0

1-[[(9H-???-9-????)???]??]-2,5-?????? C??? ??, ??, ??

??? ??

White powder

??

N-(9-Fluorenylmethoxycarbonyloxy)succinimide is used in conjunction with Isothiocyanate to conduct partial Edman Degradation on biologically active peptides.

Purification Methods

Recrystallise the carbonate from CHCl3/Et2O, or from pet ether (b 40-60o). [Pauet Can J Chem 60 976 1982, Lapatsaris et al. Synthesis 671 1983.]

1-[[(9H-???-9-????)???]??]-2,5-?????? ?? ?? ? ???

???

?? ??

Fmoc-8-amino-3,6-dioxaoctanoic acid FMOC-L-??????? FMOC-b-Ala-OH Fmoc-Leu-OH FMOC-D-PHG-OH Fmoc-L-4-Iodophenylalanine Fmoc-4-???-L-????? FMOC-L-???? Fmoc-Cys(tBu)-OH N-Boc-N'-Fmoc-L-Lysine Fmoc-L-???????? FMOC-(2S,3R)-2-AMINO-3-HYDROXY-4-METHYLPENTANOIC ACID Piperidine, 1-(9H-fluoren-9-ylmethyl)- FMOC-2-(2-AMINOETHOXY)ETHANOL N-Fmoc-L-homoserine Nalpha-FMOC-L-Tryptophan FMOC-L-Methionine

1-[[(9H-???-9-????)???]??]-2,5-?????? ?? ??

???( 726)?? ??
??? ?? ??? ?? ?? ? ??
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1-[[(9H-???-9-????)???]??]-2,5-?????? ?? ??:

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