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31138-65-5
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Sodium glucoheptonate
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SODIUM HEPTAGLUCONATE;Sodium Glucoheptonate Dihydrate;GAL[2346AC]Β(1-3)GLCN3[46BZD]-Β-MP;Squalane 111-01-3;LacMP 4'-OH, per OBn;LacMP 3'-OH, per OBn;Natriumglucoheptonat;SODIUM GLUCOHEPTONATE;SODIUM GLUCO HEPTANATE;SODIUM A-GLUCOHEPTONATE
CBNumber:
CB7430675
???:
C7H15NaO8
??? ??:
250.18
MOL ??:
31138-65-5.mol

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177 °C
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117℃[at 101 325 Pa]
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1.45[at 20℃]
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132.5 ° (C=1, H2O)
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Inert atmosphere,Store in freezer, under -20°C
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DMSO: 50 mg/mL (175.94 mM);Ethanol: Insoluble
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LogP
-6.44 at 20℃
CAS ??????
31138-65-5(CAS DataBase Reference)
EPA
D-gluco-Heptonic acid, monosodium salt, (2.xi.)- (31138-65-5)
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  • ?? ? ???? ?? (GHS)
????? 24/25
WGK ?? 3
TSCA Yes
HS ?? 2918.19.9000
???? ?? KE-17662
????(GHS): GHS hazard pictograms
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H303 ??? ??? ? ?? ?? ?? ?? - ?? ?? 5 P312
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P270 ? ??? ??? ??? ???, ???? ???? ???.
P301+P312 ??? ???? ??? ????(??)? ??? ????.
P403 ??? ? ?? ?? ?????.

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Sodium glucoheptonate is used for cleaning metal, mercerizing, paint stripping, and aluminum etching. It is also used to mercerize cotton, linen, hemp, and other plant-based fibers to increase strength and add luster to their overall appearance of threads and fabrics.

Synthesis

98 g (2 mol) of sodium cyanide and 300 g of water were charged into a flask fitted with a stirrer, thermometer and a connection to a water jet aspirator. The contents of the flask were cooled to 2 ℃. using an ice bath. 396 g (2 mol) of dextrose hydrate were charged into the flask over about 30 minutes. When the sugar had all been charged, the temperature rose to 8 ℃., when the vacuum jet was turned on to provide a vacuum of about 40 mm of Hg. Within about 30 minutes, the temperature rose to 27 ℃., when the ammonia began to boil off vigorously. Within approximately 1 hour, the alpha sodium glucoheptonate dihydrate began to crystallize. The removal of the ammonia was continued at 27 ℃ and a vacuum of 33-40 mm of Hg for 6 hours. The crystals were filtered, water washed, and air dried. The first crop yield of alpha sodium glucoheptonate was -328 grams or 57.7% of the theoretical.

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