ChemicalBook >?? ???? >Creatine ethyl ester hydrochloride
Creatine ethyl ester hydrochloride
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Creatine ethyl ester hydrochloride ??
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- 162-165°C
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- under inert gas (nitrogen or Argon) at 2-8°C
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- ?? ? ???? ?? (GHS)
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Creatine ethyl ester hydrochloride C??? ??, ??, ??
Synthesis
Creatine ethyl ester hydrochloride is prepared by the reaction of ethanol and creatine. The specific synthesis steps are as follows:Phosphorochloridic acid (2.0-2.5 equivalents to creatine) was added dropwise to a suspension of creatine in 10 mL of ethanol at 0° C. The reaction mixture was stirred for 15 min at 0° C. and the temperature then raised to 60° C. and stirred for 30 min. The reaction mixture was then cooled to provide 1.7 g of the hydrochloride salt of title compound (24) (73percent yield) as a white solid. 1H NMR (CD3OD, 400 MHz): δ 4.20-4.30 (m, 4H), 3.16(s, 3H, creatinine NCH3), 3.08 (s, 3H, CBE NCH3), 1.31 (d, J=6.8 Hz), (CBE/creatinine=9:1).
Creatine ethyl ester hydrochloride ?? ?? ? ???
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Creatine ethyl ester hydrochloride ?? ??
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Creatine ethyl ester hydrochloride ?? ??:
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L-Arginine ethyl ester dihydrochloride
Tris(trimethylsilyl)phosphate
Creatine Phosphokinase
Creatine HCL
Ethyl nipecotate
Topotecan hydrochloride
Ethyl sarcosinate hydrochloride
CreatineGluconate
Creatine ethyl ester hydrochloride
BUTTPARK 111\40-77
BUTTPARK 111\40-62
BUTTPARK 111\40-60