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2,6-????-4-?????

2,6-????-4-?????
2,6-????-4-????? ??? ???
?? ??:
99-28-5
???:
2,6-????-4-?????
???(??):
2,6-????-4-?????
???:
2,6-Dibromo-4-nitrophenol
???(??):
2,6-Dibromo-4-nit;2,6-DibroMo-4-nitrop;2,6-Dibromo-4-mitrophenol;2,6-DIBROMO-4-NITROPHENOL;4-Nitro-2,6-dibromophenol;2,6-dibromo-4-nitro-pheno;Benzbromarone Impurity 16;Dibromo-4-nitrophenol, 2,6-;Phenol, 2,6-dibromo-4-nitro-;2,6-dibromo-4-nitrophenolate
CBNumber:
CB0706661
???:
C6H3Br2NO3
??? ??:
296.9
MOL ??:
99-28-5.mol

2,6-????-4-????? ??

???
145 °C (dec.)(lit.)
?? ?
297.8±40.0 °C(Predicted)
??
2.3436 (rough estimate)
???
1.6220 (estimate)
?? ??
2-8°C(protect from light)
??? ??
powder to crystal
?? ?? (pKa)
3.67±0.44(Predicted)
??
White to Orange to Green
BRN
1245050
InChIKey
WBHYZUAQCSHXCT-UHFFFAOYSA-N
CAS ??????
99-28-5(CAS DataBase Reference)
NIST
2,6-Dibromo-4-nitrophenol(99-28-5)
EPA
2,6-Dibromo-4-nitrophenol (99-28-5)
??
  • ?? ? ?? ??
  • ?? ? ???? ?? (GHS)
??? ?? Xn,C
?? ???? ?? 20/21/22-36/37/38
????? 26-36-37
WGK ?? 3
RTECS ?? SK8025000
TSCA Yes
HS ?? 29089990
????(GHS): GHS hazard pictograms
?? ?: Warning
??·?? ??:
?? ??·?? ?? ?? ?? ?? ?? ? ?? ?? P- ??
H315 ??? ??? ??? ????? ?? ????? ?? 2 ?? GHS hazard pictograms P264, P280, P302+P352, P321,P332+P313, P362
H319 ?? ?? ??? ??? ?? ? ?? ?? ??? ?? ?? 2A ?? GHS hazard pictograms P264, P280, P305+P351+P338,P337+P313P
H335 ?? ???? ??? ? ?? ?? ???? ?? - 1? ??;???? ?? ?? 3 ?? GHS hazard pictograms
H401 ????? ??? ?? ????? ?? - ?? ?? 2 P273, P501
??????:
P261 ??·?·??·???·??·...·????? ??? ????.
P264 ?? ??? ?? ??? ????.
P264 ?? ??? ?? ??? ????.
P270 ? ??? ??? ??? ???, ???? ???? ???.
P271 ?? ?? ??? ? ?? ???? ?????.
P273 ???? ???? ???.
P280 ????/???/???/?????? ?????.
P304+P340 ???? ??? ??? ?? ??? ??? ???? ?? ??? ??? ????.
P305+P351+P338 ?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.
P405 ???? ?????.
P501 ...? ??? / ??? ?? ???.
NFPA 704
0
2 0

2,6-????-4-????? C??? ??, ??, ??

??? ??

yellow crystalline powder

Purification Methods

Crystallise the phenol from aqueous EtOH, 50% aqueous AcOH (m 144-145o, dec varies with rate of heating). Dry it in an oven at 40-60o or in vacuo over NaOH. [Hartman & Dickey Org Synth Coll Vol II 173 1943, Beilstein 6 H 246, 6 I 123, 6 II 234, 6 III 849, 6 IV 1366.]

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