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2,4-DINITROBENZENESULFONYL CHLORIDE

2,4-DINITROBENZENESULFONYL CHLORIDE ??? ???
?? ??:
1656-44-6
???:
2,4-DINITROBENZENESULFONYL CHLORIDE
???(??):
2,4-DinitrobenzenesuL;2,4-Dinitrobenzenesulfonylchl;4-Dinitrobenzenesulfonyl chloride;2,4-Dinitrophenylsulfonyl chloride;2,4-dinitro-benzenesulfonylchlorid;2,4-DINITROBENZENESULFONYL CHLORIDE;2,4-DINITROBENZENESULPHONYL CHLORIDE;Benzenesulfonyl chloride, 2,4-dinitro-;1-(Chlorosulphonyl)-2,4-dinitrobenzene;2,4-Dinitrobenzenesulfonyl chloride,98%
CBNumber:
CB0472238
???:
C6H3ClN2O6S
??? ??:
266.62
MOL ??:
1656-44-6.mol
MSDS ??:
SDS

2,4-DINITROBENZENESULFONYL CHLORIDE ??

???
101-103 °C (lit.)
?? ?
60-80 °C
??
1.780
?? ??
-20°C Freezer
???
?????(?? ???)
??? ??
??
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??? ??
??
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Moisture Sensitive
BRN
2147583
???
???
CAS ??????
1656-44-6(CAS DataBase Reference)
EPA
Benzenesulfonyl chloride, 2,4-dinitro- (1656-44-6)
??
  • ?? ? ?? ??
  • ?? ? ???? ?? (GHS)
??? ?? T,C
?? ???? ?? 34-65-48/23/24/25-46-45-48/20/21/22
????? 53-26-36/37/39-45-62
????(UN No.) UN 3261 8/PG 2
WGK ?? 3
F ?????? 21
TSCA Yes
?? ?? 8
???? II
HS ?? 2904990090
????(GHS): GHS hazard pictogramsGHS hazard pictograms
?? ?: Danger
??·?? ??:
?? ??·?? ?? ?? ?? ?? ?? ? ?? ?? P- ??
H314 ??? ?? ??? ?? ??? ??? ????? ?? ????? ?? 1A, B, C ?? GHS hazard pictograms P260,P264, P280, P301+P330+ P331,P303+P361+P353, P363, P304+P340,P310, P321, P305+ P351+P338, P405,P501
H340 ???? ??? ??? ? ?? (????? ???? ????? ???? ???? ???? ??? ?? ????? ??? ???? ??) ???? ???? ?? ?? 1A, 1B ?? GHS hazard pictograms
H350 ?? ??? ? ?? (????? ?? ???? ???? ???? ??? ?? ????? ??? ???? ??) ??? ?? ?? 1A, 1B ?? GHS hazard pictograms
H373 ??? ?? ?? ???? ??(??, ??? ?? ??? ?? ??? ??)? ??? ??? ? ?? ?? ???? ?? - ?? ?? ?? 2 ?? P260, P314, P501
??????:
P202 ?? ?? ?? ??? ?? ???? ??? ???? ???.
P260 ??·?·??·???·??·...·????? ???? ???.
P280 ????/???/???/?????? ?????.
P303+P361+P353 ??(?? ????)? ??? ??? ?? ??? ??? ????? ??? ?? ????/?????.
P305+P351+P338 ?? ??? ? ?? ?? ???? ????. ???? ?????? ?????. ?? ????.
NFPA 704
1
3 0

2,4-DINITROBENZENESULFONYL CHLORIDE C??? ??, ??, ??

??? ??

yellow crystalline powder

??

2,4-Dinitrobenzenesulfonyl chloride was used to protect primary amines. It was used as starting reagent in the synthesis of tert-butyl 2-[(2,4-dinitrophenyl) sulfonyl]amino acetate.

?? ??

2,4-Dinitrobenzenesulfonyl chloride causes the sulfonation of glycosylamines to yield N-glycosyl-2,4-dinitrobenzenesulfonamides.

Purification Methods

Crystallise the sulfonyl chloride from *benzene or *benzene/pet ether. [Beilstein 11 H 78, 11 IV 214.]

2,4-DINITROBENZENESULFONYL CHLORIDE ?? ?? ? ???

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2,4-DINITROBENZENESULFONYL CHLORIDE ?? ??:

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