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Tiaramid

Tiaramide Struktur
32527-55-2
CAS-Nr.
32527-55-2
Bezeichnung:
Tiaramid
Englisch Name:
Tiaramide
Synonyma:
NTA-194;Tiaramida;Rhc 2592a;Tiaramide;Brn 1030245;Einecs 251-083-7;Tiaramide USP/EP/BP;35941-71-0 (Mono-hydrochloride);4-[(5-Chloro-2-oxobenzothiazol-3-yl)acetyl]-1-piperazineethanol;4-((5-Chloro-2-oxo-3(2H)-benzothiazolyl)acetyl)-1-piperazineethanol
CBNumber:
CB8875246
Summenformel:
C15H18ClN3O3S
Molgewicht:
355.84
MOL-Datei:
32527-55-2.mol

Tiaramid Eigenschaften

Schmelzpunkt:
159-161 °C
Siedepunkt:
605.8±65.0 °C(Predicted)
Dichte
1.432±0.06 g/cm3(Predicted)
pka
6.2(at 25℃)

Sicherheit

Tiaramid Chemische Eigenschaften,Einsatz,Produktion Methoden

Originator

Solantal,Fujisawa,Japan,1975

Manufacturing Process

A solution of ethyl 5-chloro-2-oxo-3-benzo-thiazolineacetate (4.0 grams) in 1- (2-hydroxyethyl)piperazine is heated at 100°C for 24 hours. After cooling, the resulting mixture is extracted with chloroform. The chloroform extract is washed with water and shaken with 10% hydrochloric acid. The hydrochloric acid layer is washed with chloroform, made alkaline with 10% sodium hydroxide solution and extracted with chloroform. The chloroform extract is washed with water, dried over magnesium sulfate and concentrated. The residual oil (5.5 grams) is allowed to stand to form crystals, which are recrystallized from a mixture of ethyl acetate (40 ml) and ethanol (15 ml) to give 3-[4-(2-hydroxyethyl)-1-piperazinylcarbonylmethyl]-5-chloro-2(3H)- benzothiazolinone (3.2 grams) as colorless crystals, MP 159° to 161°C. The following is an alternate method of preparation: A mixture of 3-(1- piperazinyl)carbonylmethyl-5-chloro-2(3H)-benzothiazolinone (500 mg), anhydrous potassium carbonate (400 mg), 2-hydroxyethyl bromide (300 mg) and anhydrous ethanol (20 ml) is heated while refluxing for 5 hours. The reaction mixture is concentrated under reduced pressure. The residue is extracted with chloroform. The chloroform layer is dried over magnesium sulfate and concentrated. The residue is crystallized from a mixture of ethyl acetate and ethanol to give 3-[4-(2-hydroxyethyl]-1- piperazinylcarbonylmethyl]-5-chloro-2(3H)-benzothiazolinone (370 mg) as crystals, MP 159° to 160°C.

Therapeutic Function

Antiinflammatory

Tiaramid Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Tiaramid Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 9)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
CONIER CHEM AND PHARMA LIMITED
+8618523575427
sales@conier.com China 49374 58
Dideu Industries Group Limited
+86-29-89586680 +86-15129568250
1026@dideu.com China 22787 58
Chengdu Kamel Pharmaceutical Co., Ltd 028-67136579 15828051124
sales@kamelpharm.com China 1912 55
Bide Pharmatech Ltd. 400-1647117 13681763483
product02@bidepharm.com China 62075 58
Bide Pharmatech Ltd. 400-6005915
sales@picasso-e.com China 39653 58
Shanghai Jieshikai Biotechnology Co. , Ltd. 021-57520305 15221441005
wangkang@jskchem.com China 49234 58

32527-55-2(Tiaramid)Verwandte Suche:


  • 1-Piperazineethanol, 4-((5-chloro-2-oxo-3(2H)-benzothiazolyl)acetyl)- (9ci)
  • 1-Piperazineethanol, 4-((5-chloro-2-oxo-3-benzothiazolinyl)acetyl)-
  • 35941-71-0 (Mono-hydrochloride)
  • 4-((5-Chloro-2-oxo-3(2H)-benzothiazolyl)acetyl)-1-piperazineethanol
  • 5-Chlor-2,3-dihydro-3-(4-(2-hydroxyethyl)piperazinylcarbonylmethyl)-2-benzothiazolon
  • Brn 1030245
  • Einecs 251-083-7
  • Rhc 2592a
  • Tiaramida
  • 4-[(5-Chloro-2-oxobenzothiazol-3-yl)acetyl]-1-piperazineethanol
  • 5-Chloro-3-[[4-(2-hydroxyethyl)-1-piperazinyl]carbonylmethyl]-2,3-dihydrobenzothiazol-2-one
  • NTA-194
  • 4-[(5-Chloro-2-oxo-3(2H)-benzothiazolyl)acetyl]piperazine-1-ethanol
  • Tiaramide
  • 2(3H)-Benzothiazolone, 5-chloro-3-[2-[4-(2-hydroxyethyl)-1-piperazinyl]-2-oxoethyl]-
  • Tiaramide USP/EP/BP
  • 32527-55-2
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