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N2,N6-Dibenzyloxycarbonyl-L-lysin

Z-Lys(Z)-OH  Struktur
405-39-0
CAS-Nr.
405-39-0
Bezeichnung:
N2,N6-Dibenzyloxycarbonyl-L-lysin
Englisch Name:
Z-Lys(Z)-OH
Synonyma:
Z-Lys;CBZ-LYS(CBZ)-OH;Cbz-Lys(Z)-OH;Z-LYS(Z);NSC 88474;Z-LYS(Z)-OH;Z-L-Lys(Z)-OH;Z-LYSINE(Z)-OH;DI-N-CBZ-L-LYSINE;Cbz-L-Lys(Cbz)-OH
CBNumber:
CB7208816
Summenformel:
C22H26N2O6
Molgewicht:
414.45
MOL-Datei:
405-39-0.mol

N2,N6-Dibenzyloxycarbonyl-L-lysin Eigenschaften

Schmelzpunkt:
76-78°C
Siedepunkt:
659.0±55.0 °C(Predicted)
Dichte
1.238±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
L?slichkeit
DMSO (Slightly), Methanol (Slightly)
Aggregatzustand
Solid
pka
3.97±0.21(Predicted)
Farbe
White to Off-White
BRN 
1897206
InChIKey
BLZXFNUZFTZCFD-IBGZPJMESA-N
SMILES
C(O)(=O)[C@H](CCCCNC(OCC1=CC=CC=C1)=O)NC(OCC1=CC=CC=C1)=O
CAS Datenbank
405-39-0(CAS DataBase Reference)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
WGK Germany  3
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H302 Gesundheitssch?dlich bei Verschlucken. Akute Toxizit?t oral Kategorie 4 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P270, P301+P312, P330, P501
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizit?t (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" />
Sicherheit
P261 Einatmen von Staub vermeiden.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

N2,N6-Dibenzyloxycarbonyl-L-lysin Chemische Eigenschaften,Einsatz,Produktion Methoden

Chemische Eigenschaften

White Solid

Verwenden

Protected L-lysine

Definition

Z-Lys(Z)-OH is a lysine derivative.

Synthese

A 250 mL three-necked flask was loaded consecutively with water (20 mL), 1,4-dioxane (20 mL), and L-lysine (2.1 g, 14.4 mmol). The mixture was stirred until complete dissolution. The pH was adjusted to about 10.5 by the addition of 30% NaOH. Benzyl chloroformate (5.2 g, 30.6 mmol) was added while maintaining the pH at about 1011 by adding at the same time 30% NaOH. At the end of the addition, the reaction was stirred at 20° C. for about 1 hour. The pH was adjusted to 5 with 37% HCl. Ethyl acetate (30 mL) was added and the pH was adjusted to 1 with 37% HCl. The mixture was stirred at room temperature for about 30 minutes, the organic layer was separated and the aqueous layer was extracted with ethyl acetate (20 mL). The combined organic layer was washed with brine (30 mL) and dried over Na2SO4. Then, the solvent was evaporated to yield Z-Lys(Z)-OH as a yellowish oil (6.0 g, 99%).

N2,N6-Dibenzyloxycarbonyl-L-lysin Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


N2,N6-Dibenzyloxycarbonyl-L-lysin Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 208)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Sichuan HongRi Pharma-Tech Co.,Ltd
+86-028-64841719 +8617390183901
daisy@enlaibio.com China 1106 58
Capot Chemical Co.,Ltd.
+86-(0)57185586718 +86-13336195806
sales@capot.com China 29791 60
Henan Tianfu Chemical Co.,Ltd.
+86-0371-55170693 +86-19937530512
info@tianfuchem.com China 21634 55
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795
ivan@atkchemical.com China 32957 60
AB PharmaTech,LLC
323-480-4688
sales@acrospharmatech.com United States 989 55
Shenzhen Nexconn Pharmatechs Ltd
+86-755-89396905 +86-15013857715
admin@nexconn.com China 10311 58
Xiamen AmoyChem Co., Ltd
+86-86-5926051114 +8618959220845
sales@amoychem.com China 6383 58
Alchem Pharmtech,Inc.
8485655694
sales@alchempharmtech.com United States 63687 58
career henan chemical co
+86-0371-86658258 +8613203830695
factory@coreychem.com China 29811 58
SIMAGCHEM CORP
+86-13806087780
sale@simagchem.com China 17365 58

405-39-0(N2,N6-Dibenzyloxycarbonyl-L-lysin)Verwandte Suche:


  • DI-N-CBZ-L-LYSINE
  • DICARBOBENZOXY-L-LYSINE
  • Z-LYSINE(Z)-OH
  • Z-LYS(Z)-OH
  • N-ALPHA,EPSILON-BIS-Z-L-LYSINE
  • N-ALPHA,N-EPSILON-DI-Z-L-LYSINE
  • N-ALPHA, N-EPSILON-DIBENZYLOXYCARBONYL-L-LYSINE
  • N-ALPHA-N-EPSILON-DICARBOBENZOXY-L-LYSINE
  • N-ALPHA-N-EPSILON-DI-CBZ-L-LYSINE
  • N,N'-DI-CBZ-L-LYSINE
  • di-N-CBZ-L-Lysine di-N-Carbobenzyloxy-L-lysine
  • Cbz-L-Lys(Cbz)-OH
  • Nα,ε-Bis-Z-L-lysine≥ 99% (HPLC)
  • N,N-di-cbz-L-lysine free acid
  • N2,N6-dibenzyloxycarbonyl-L-lysine
  • NA,NE-DIBENZYLOXYCARBONYL-L-LYSINE
  • Z-LYS(Z)
  • L-Lysine, N2,N6-bis[(phenylmethoxy)carbonyl]-
  • N1,N6-DI-CBZ-L-LYSINE
  • N,N'-di-carbobenzyloxy-L-lysine
  • N,Nμ-Di-Cbz-L-lysine, Nα,Nε-Di-Z-L-lysine
  • N2,N6-Bis(benzyloxycarbonyl)-L-lysine
  • N2,N6-Bis(benzyloxycarbonyl)lysine
  • N2,N6-Bis[(benzyloxy)carbonyl]-L-lysine
  • Nα,Nε-Bis(benzyloxycarbonyl)-L-lysine
  • N,N'-Dibenzyloxycarbonyl-L-lysine
  • N-alpha-N-epsilon-Bis-benzyloxycarbonyl-L-lysine
  • Z-L-Lys(Z)-OH
  • N-beta,epsilon-Bis-Z-L-lysine
  • N,N'-(Dicarobenzyloxy)-L-lysine
  • N2,N6-Bis[(phenylMethoxy)carbonyl]-L-lysine
  • N2,N6-Dicarbobenzoxy-L-lysine
  • NSC 88474
  • N2,N6-Bis-Cbz-L-lysine
  • ZzLys[Z-Lys(Z)-OH]
  • (S)-2,6-Bis(((benzyloxy)carbonyl)aMino)hexanoic acid
  • Z-Lys(Z)-OH, 98%+
  • Z-Lys(Z)-OH >=98.0% (TLC)
  • TIANFUCHEM--405-39-0--High purity Z-LYS(Z)-OH factory price
  • Nα,ε-Bis-Z-L-lysine
  • Z-LYS(Z)-OH USP/EP/BP
  • (2S)-2,6-bis(phenylmethoxycarbonylamino)hexanoicaci
  • (2S)-2,6-di{[(benzyloxy)carbonyl]amino}hexanoic acid
  • (2S)-2,6-bis(phenylmethoxycarbonylamino)hexanoic acid
  • Cbz-Lys(Z)-OH
  • CBZ-LYS(CBZ)-OH
  • Nα,Nε-Di-Z-L-lysine
  • N2,N6-Dibenzyloxycarbonyl-L-lysin
  • Z-Lys
  • N,N'-Dibenzyloxycarbonyl-L-lysine
  • 405-39-0
  • C6H5CH2O2CNHCH24CHNHCO2CH2C6H5CO2H
  • CARBOXYLIC ACID
  • Peptide Synthesis
  • Specialty Synthesis
  • Lysine
  • Amino Acid Derivatives
  • Amino Acid Derivatives
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