2-Bromo-N,N-diphenylaniline
|
|
|
- CAS-Nr.
- 78600-31-4
- Englisch Name:
- 2-Bromo-N,N-diphenylaniline
- Synonyma:
- 2-BTPA;2-Bromophenyldipheny;2-BroMo TriphenylaMine;2-Bromotriphenylamine >2-Bromophenyldiphenylamine;o-Bromophenyldiphenylamine;2-BroMo-N,N-diphenylaniline;9-(2-broMophenyl) Carbazole;2-bromo-N,N-diphenylbenzenamine;Benzenamine, 2-bromo-N,N-diphenyl-
- CBNumber:
- CB62610599
- Summenformel:
- C18H14BrN
- Molgewicht:
- 324.21
- MOL-Datei:
- 78600-31-4.mol
|
2-Bromo-N,N-diphenylaniline Eigenschaften
- Schmelzpunkt:
- 61.0 to 65.0 °C
- Siedepunkt:
- 165°C/0.3mmHg(lit.)
- Dichte
- 1.369
- storage temp.
- Sealed in dry,Room Temperature
- L?slichkeit
- soluble in Toluene
- Aggregatzustand
- powder to crystal
- pka
- -3.76±0.18(Predicted)
- Farbe
- White to Almost white
- InChIKey
- YPIANBZIVBPMJS-UHFFFAOYSA-N
2-Bromo-N,N-diphenylaniline Chemische Eigenschaften,Einsatz,Produktion Methoden
Synthese
Diphenylamine (1.6900 g, 10.0 mmol), o-dibromobenzene (2.40 mL, 20.0 mmol), copper iodide (0.1900 g, 1.0 mmol), 18-crown-6 (0.1320 g, 0.5 mmol), and 60 mL of o-dichlorobenzene were sequentially added to the reaction flask. Under nitrogen protection and dark conditions, stir and heat to 100-210°C for 5-100 hours. Stop the reaction and slowly reduce to room temperature, vacuum distillation of most of the solvent, and suction filtration; the solid residue is washed with dichloromethane solution, and the organic phases are combined. Concentration and column chromatography gave 2-Bromo-N, N-diphenylamine (yield: 73 per cent).
2-Bromo-N,N-diphenylaniline Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
2-Bromo-N,N-diphenylaniline Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.
Global( 151)Lieferanten
78600-31-4()Verwandte Suche:
- 2-BroMo TriphenylaMine
- 9-(2-broMophenyl) Carbazole
- o-Bromophenyldiphenylamine
- 2-BroMo-N,N-diphenylaniline
- 2-BTPA
- 2-bromo-N,N-diphenylbenzenamine
- Benzenamine, 2-bromo-N,N-diphenyl-
- 2-Bromophenyldiphenylamine
- 2-Bromophenyldipheny
- N-(2-bromophenyl)-N-phenylbenzenamine
- 2-Bromotriphenylamine >
- 78600-31-4
- OLED
