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N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE Struktur
80376-66-5
CAS-Nr.
80376-66-5
Englisch Name:
N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE
Synonyma:
meyers' tms form;N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE;N-Methyl-N-trimethylsilylmethyl-N'-tert-butylformamidine,98%;N'-tert-butyl-N-methyl-N-(trimethylsilylmethyl)methanimidamide;Methanimidamide, N'-(1,1-dimethylethyl)-N-methyl-N-[(trimethylsilyl)methyl]-;N-Methyl-N-trimethylsilylmethyl-N'-tert-butylformamidineMeyers' TMS form reagent
CBNumber:
CB6160140
Summenformel:
C10H24N2Si
Molgewicht:
200.4
MOL-Datei:
80376-66-5.mol

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE Eigenschaften

Siedepunkt:
78-80 °C (7 mmHg)
Brechungsindex
1.45-1.452
storage temp. 
0-6°C

Sicherheit

Kennzeichnung gef?hrlicher Xn
R-S?tze: 20/21/22
S-S?tze: 36/37

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R20/21/22:Gesundheitssch?dlich beim Einatmen,Verschlucken und Berührung mit der Haut.

S-S?tze Betriebsanweisung:

S36/37:Bei der Arbeit geeignete Schutzhandschuhe und Schutzkleidung tragen.

Chemische Eigenschaften

CLEAR PALE YELLOW LIQUID

Verwenden

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE conveniently effects the transformation of ketones and aldehydes to homologated nitriles, amines, aldehydes, and ketones.

Synthese

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE is easily synthesized by a two-step procedure (eq 1).1 Initially, the condensation of t-Butylamine with either N,N-Dimethylformamide or dimethylformamide dimethyl acetal cleanly affords N′-t-Butyl-N,N-dimethylformamidine. Subsequent lithiation and silylation with Chlorotrimethylsilane results in a 70% overall yield of the purified title reagent.
N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE synthesis route

Lager

The reagent should be handled in a fume hood. Refrigeration should be used for prolonged storage.

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 4)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Acros Organics --
 info@acros.com Belgium 6772 81
3B Scientific Corporation --
 sales@3bsc.com United States 6718 47
Service Chemical Inc. --
 sales@chemos-group.com Germany 6350 71
Kanto Chemical Co., Inc. --
 reag-info@gms.kanto.co.jp Japan 6756 74

80376-66-5()Verwandte Suche:

  • meyers' tms form
  • N-Methyl-N-trimethylsilylmethyl-N'-tert-butylformamidine,98%
  • N-Methyl-N-trimethylsilylmethyl-N'-tert-butylformamidineMeyers' TMS form reagent
  • N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE
  • Methanimidamide, N'-(1,1-dimethylethyl)-N-methyl-N-[(trimethylsilyl)methyl]-
  • N'-tert-butyl-N-methyl-N-(trimethylsilylmethyl)methanimidamide
  • 80376-66-5
  • C10H24N2Si
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