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1-Bromo-4-(pentafluorosulfanyl)benzene

1-Bromo-4-(pentafluorosulfanyl)benzene Struktur
774-93-6
CAS-Nr.
774-93-6
Englisch Name:
1-Bromo-4-(pentafluorosulfanyl)benzene
Synonyma:
(4-Bromophenyl)pentafluoro-l6-sulfane;4-BROMOPHENYLSULFUR PENTAFLUORIDE;4-BROMOPHENYL-PENTAFLUOROSULFUR;4-Pentafluorosulfur bromobenzene;p-Bromophenylsulfur Pentafluoride;4-BROMOPHENYLSULPHUR PENTAFLUORIDE;1-BROMO-4-(PENTAFLUOROTHIO)BENZENE;4-Bromophenylsulfur Pentafluoride >1-BROMO-4-(PENTAFLUOROSULFANYL)BENZENE;4-BroMophenylsulfur pentafluoride, 95+%
CBNumber:
CB5263002
Summenformel:
C6H4BrF5S
Molgewicht:
283.06
MOL-Datei:
774-93-6.mol

1-Bromo-4-(pentafluorosulfanyl)benzene Eigenschaften

Siedepunkt:
77.2 °C(Press: 10 Torr)
Brechungsindex
1.4790-1.4830
Flammpunkt:
84°C(lit.)
storage temp. 
0-10°C
Aggregatzustand
liquid
Farbe
Clear, colourless
InChI
InChI=1S/C6H4BrF5S/c7-5-1-3-6(4-2-5)13(8,9,10,11)12/h1-4H
InChIKey
RECCABBXFXGELM-UHFFFAOYSA-N
SMILES
S(F)(F)(F)(F)(F)C1=CC=C(Br)C=C1
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher Xi
R-S?tze: 20/21/22-36/37/38
S-S?tze: 23-26-36/37/39
Hazard Note  Irritant
HS Code  2930909899
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H227 Combustible liquid Flammable liquids Category 4 Warnung P210, P280, P370+P378, P403+P235,P501
H302 Gesundheitssch?dlich bei Verschlucken. Akute Toxizit?t oral Kategorie 4 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P270, P301+P312, P330, P501
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
Sicherheit
P210 Von Hitze, hei?en Oberfl?chen, Funken, offenen Flammen und anderen Zündquellenarten fernhalten. Nicht rauchen.
P264 Nach Gebrauch gründlich waschen.
P264 Nach Gebrauch gründlich waschen.
P270 Bei Gebrauch nicht essen, trinken oder rauchen.
P280 Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.
P403+P235 An einem gut belüfteten Ort aufbewahren. Kühl halten.

1-Bromo-4-(pentafluorosulfanyl)benzene Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

5.0 g of 4-pentafluorosulfanylaniline was dissolved in 20 ml of acetic acid, and, at 0 ℃, a saturated aqueous HBr solution was added. Then, at 0 ℃, a solution of 1.9 of NaNO2 in 5 ml of water was slowly added dropwise over the course of 5 minutes. The reaction mixture was stirred at 0 C. for 10 minutes and then added in portions to a suspension of 6.5 g of CuBr in 20 ml of a half-saturated aqueous HBr solution at 0 ℃. Nitrogen is liberated during this. The mixture was stirred at 0 ℃. for 30 minutes and then at RT for 1 h. It was subsequently extracted 3 times with 100 ml of HEP each time, and then the HEP was washed twice with 50 ml of a saturated aqueous Na2CO3 solution each time. The residue, after drying over MgSO4 and removal of the solvent in vacuo, was chromatographed on silica gel with HEP. 1.8 g of a colorless oil 1-Bromo-4-(pentafluorosulfanyl)benzene were obtained.

1-Bromo-4-(pentafluorosulfanyl)benzene Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

[4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]sulfur pentafluoride

1-Bromo-4-(pentafluorosulfanyl)benzene Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

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774-93-6()Verwandte Suche:

  • 4-BROMOPHENYL-PENTAFLUOROSULFUR
  • 4-BROMOPHENYLSULPHUR PENTAFLUORIDE
  • 1-BROMO-4-(PENTAFLUOROSULFANYL)BENZENE
  • 1-BROMO-4-(PENTAFLUOROTHIO)BENZENE
  • 4-Pentafluorosulfur bromobenzene
  • 1-Bromo-4-(pentafluorothio)benzene, 1-Bromo-4-(pentafluorosulphanyl)benzene
  • 4-BroMophenylsulfur pentafluoride, 95+%
  • Sulfur,(4-broMophenyl)pentafluoro-, (OC-6-21)- (9CI)
  • Sulfur, (4-bromophenyl)pentafluoro-, (OC-6-21)-
  • 4-Bromophenylsulfur Pentafluoride >
  • p-Bromophenylsulfur Pentafluoride
  • 4-BROMOPHENYLSULFUR PENTAFLUORIDE
  • (4-Bromophenyl)pentafluoro-l6-sulfane
  • (OC-6-21)-(4-Bromophenyl)pentafluorosulfur
  • (4-bromophenyl)-pentafluoro-lambda6-sulfane
  • 774-93-6
  • C6H4F5BrS
  • Halides
  • Phenyls & Phenyl-Het
  • Phenyls & Phenyl-Het
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