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4-IODOBUTYL ACETATE

4-IODOBUTYL ACETATE Struktur
40596-44-9
CAS-Nr.
40596-44-9
Englisch Name:
4-IODOBUTYL ACETATE
Synonyma:
4-IODOBUTYL ACETATE;1-ACETOXY-4-IODOBUTANE;4-iodobutyl acetate 96%;4-ACETOXY-BUTAN-1-IODIDE;4-iodo-1-butanol acetate;1-Butanol, 4-iodo-, 1-acetate;4-Iodobutylacetate, 85%, tech.;4-Iodobutyl acetate, 97%, stab;ACETIC ACID 4-IODO-BUTYL ESTER;4-IODOBUTYL ACETATE, TECH., 85%
CBNumber:
CB1210301
Summenformel:
C6H11IO2
Molgewicht:
242.05
MOL-Datei:
40596-44-9.mol

4-IODOBUTYL ACETATE Eigenschaften

Siedepunkt:
94-95 °C5.5 mm Hg(lit.)
Dichte
1.61 g/mL at 25 °C(lit.)
Brechungsindex
n20/D 1.497(lit.)
Flammpunkt:
195 °F
L?slichkeit
Difficult to mix.
Aggregatzustand
liquid
Farbe
Light green turbid
Sensitive 
Light Sensitive
CAS Datenbank
40596-44-9(CAS DataBase Reference)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher Xi
R-S?tze: 36/37/38
S-S?tze: 26-36/37/39
WGK Germany  3
HS Code  29153900
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H227 Combustible liquid Flammable liquids Category 4 Warnung P210, P280, P370+P378, P403+P235,P501
Sicherheit
P403+P235 An einem gut belüfteten Ort aufbewahren. Kühl halten.

4-IODOBUTYL ACETATE Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.

S-S?tze Betriebsanweisung:

S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.
S36/37/39:Bei der Arbeit geeignete Schutzkleidung,Schutzhandschuhe und Schutzbrille/Gesichtsschutz tragen.

Chemische Eigenschaften

CLEAR DARK BROWN LIQUID

Verwenden

4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodide

Synthesis Reference(s)

Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770

Synthese

The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.
synthesis of 4-IODOBUTYL ACETATE

4-IODOBUTYL ACETATE Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


4-IODOBUTYL ACETATE Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 59)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Hebei Mojin Biotechnology Co., Ltd
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sales@hbmojin.com China 12834 58
Hefei TNJ Chemical Industry Co.,Ltd.
+86-0551-65418671 +8618949823763
sales@tnjchem.com China 34563 58
Nanjing Triumpharm Co.,Ltd
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SUZHOU SENFEIDA CHEMICAL CO.,LTD
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sales@senfeida.com China 23046 58
Aladdin Scientific
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Amadis Chemical Company Limited
571-89925085
sales@amadischem.com China 131957 58
Mainchem Co., Ltd. +86-0592-6210733
sale@mainchem.com China 32343 55
Meryer (Shanghai) Chemical Technology Co., Ltd. 021-61259108 18621169109
market03@meryer.com China 40228 62
Alfa Aesar 400-6106006
saleschina@alfa-asia.com China 30123 84
Energy Chemical 021-021-58432009 400-005-6266
sales8178@energy-chemical.com China 44688 61

40596-44-9()Verwandte Suche:


  • 1-ACETOXY-4-IODOBUTANE
  • 4-ACETOXY-BUTAN-1-IODIDE
  • 4-IODOBUTYL ACETATE
  • 4-IODOBUTYL ACETATE, TECH., 85%
  • ACETIC ACID 4-IODO-BUTYL ESTER
  • 4-iodo-1-butanol acetate
  • 4-Iodobutylacetate, 85%, tech.
  • 4-Iodobutylacetate1-Acetoxy-4-iodobutane
  • 4-Iodobutyl acetate, 97%, stab
  • 4-Iodobutyl acetate, 97%, stab. with copper
  • 4-Iodobutyl acetate, stabilized with copper
  • 4-Iodobutyl acetate,stab. with copper
  • 1-Butanol, 4-iodo-, 1-acetate
  • 4-iodobutyl acetate 96%
  • 4-Iodobutyl acetate, 96%, stab. with copper
  • 40596-44-9
  • C6H11IO2
  • CH3CO2CH24I
  • Carbonyl Compounds
  • C6 to C7
  • Building Blocks
  • Esters
  • Organic Building Blocks
  • Building Blocks
  • C6 to C7
  • Carbonyl Compounds
  • Chemical Synthesis
  • Esters
  • Organic Building Blocks
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