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ChemicalBook--->CAS DataBase List--->7356-11-8

7356-11-8

7356-11-8 Structure

7356-11-8 Structure
IdentificationMore
[Name]

4-Methyl-3-nitrobenzoic acid methyl ester
[CAS]

7356-11-8
[Synonyms]

3-NITRO-P-TOLUIC ACID METHYL ESTER
4-METHYL-3-NITROBENZOIC ACID METHYL ESTER
METHYL 3-NITRO-4-METHYLBENZOATE
METHYL 4-METHYL-3-NITROBENZOATE
RARECHEM AL BF 0233
4-Methyl-3-Nitro Benzoic Acid Methyl Ester Methyl 4-Methyl-3-Nitro Benzoate
3-NITRO-4-METHYLBENZOICACIDMETHYLESTER
BENZOICACID,4-METHYL-3-NITRO-,METHYLESTER(9CI)
[EINECS(EC#)]

230-886-6
[Molecular Formula]

C9H9NO4
[MDL Number]

MFCD00130054
[Molecular Weight]

195.17
[MOL File]

7356-11-8.mol
Chemical PropertiesBack Directory
[Melting point ]

49-53°C
[Boiling point ]

298.0±20.0 °C(Predicted)
[density ]

1?+-.0.06 g/cm3(Predicted)
[Fp ]

110 °C
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Soluble in methanol.
[form ]

powder to crystal
[color ]

White to Light yellow
[CAS DataBase Reference]

7356-11-8(CAS DataBase Reference)
[EPA Substance Registry System]

7356-11-8(EPA Substance)
Questions And AnswerBack Directory
[Synthesis]

Methyl 4-methyl-3-nitrobenzoate is synthesized by the following steps:Acid 33 (100 g, 0.552 mol) was dissolved in MeOH (1000 ml). Conc.  H2SO4 (30 ml) was added cautiously to this solution. The mixture was  refluxed for 8 hours. Solvent was distilled off. Ice-cold water was added  to the residue. It was then extracted with EtOAc, washed with NaHCO3 solution, water, dried (anhydrous Na2SO4), filtered and concentrated in  vacuo to furnish faint yellow a solid. (91.57 g).
Safety DataBack Directory
[Hazard Codes ]

Xn
[Risk Statements ]

R22:Harmful if swallowed.
R43:May cause sensitization by skin contact.
[Safety Statements ]

S37/39:Wear suitable gloves and eye/face protection .
[WGK Germany ]

2
[TSCA ]

Yes
[HS Code ]

29163990
Raw materials And Preparation ProductsBack Directory
[Preparation Products]

Indole-6-carboxaldehyde-->1-TERT-BUTYL 6-METHYL 3-FORMYL-1H-INDOLE-1,6-DICARBOXYLATE-->6-HYDROXYMETHYLINDOLE-->Methyl 1H-indazole-6-carboxylate-->Methyl 3-amino-4-methylbenzoate-->3-Nitro-4-(2-oxo-propyl)-benzoic acid methyl ester
Hazard InformationBack Directory
[Chemical Properties]

White solid
[Uses]

Methyl 4-methyl-3-nitrobenzoate is used as pharmaceutical intermediate.
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

Methyl 4-methyl-3-nitrobenzoate, 99%(7356-11-8)
[Sigma Aldrich]

7356-11-8(sigmaaldrich)
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