Identification | Back Directory | [Name]
CARBAZOLE-N-CARBONYL CHLORIDE | [CAS]
73500-82-0 | [Synonyms]
9-(CHLOROFORMYL)CARBAZOLE N-(CHLOROCARBONYL)CARBAZOLE 9-(Chlorocarbonyl)carbazole 9-(Chloroformyl)-9H-carbazole CARBAZOLE-N-CARBONYL CHLORIDE CARBAZOLE-9-CARBONYL CHLORIDE 9H-Carbazole-9-carbonyl chloride Carbazole-9-carbonyl Chloride > 9H-Carbazole-9-carboxylic acid chloride CARBAZOLE-9-CARBONYL CHLORIDE, FOR FLUOR ESCENCE CARBAZOLE-N-CARBONYL CHLORIDE ISO 9001:2015 REACH | [Molecular Formula]
C13H8ClNO | [MDL Number]
MFCD00059689 | [MOL File]
73500-82-0.mol | [Molecular Weight]
229.66 |
Chemical Properties | Back Directory | [Melting point ]
100-104 °C
| [Boiling point ]
407.5±28.0 °C(Predicted) | [density ]
1.32±0.1 g/cm3(Predicted) | [storage temp. ]
2-8°C
| [form ]
powder to crystal | [color ]
White to Almost white | [CAS DataBase Reference]
73500-82-0 |
Hazard Information | Back Directory | [Purification Methods]
Recrystallise the acid chloride from *C6H6. If it is not very pure (presence of OH or NH bands in the IR), dissolve it in pyridine, shake it with phosgene in toluene, evaporate and recrystallise the residue. Carry out this experiment in a good fume cupboard as COCl2 is very TOXIC, and store the product in the dark. It is moisture sensitive. The amide has m 246.5-247o, and the dimethylaminoethylamide hydrochloride has m 197-198o. [Weston et al. J Am Chem Soc 75 4006 1953, Beilstein 20 III/IV 3841.] |
|
Company Name: |
Energy Chemical
|
Tel: |
021-021-58432009 400-005-6266 |
Website: |
http://www.energy-chemical.com |
Company Name: |
TCI Europe
|
Tel: |
320-37350700 |
Website: |
https://www.tcichemicals.com/de/de/index.html |
Company Name: |
TCI AMERICA
|
Tel: |
800-4238616 |
Website: |
https://www.tcichemicals.com/en/us/index.html |
|