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ChemicalBook--->CAS DataBase List--->6609-56-9

6609-56-9

6609-56-9 Structure

6609-56-9 Structure
IdentificationMore
[Name]

2-Methoxybenzonitrile
[CAS]

6609-56-9
[Synonyms]

2-CYANOANISOLE
2-METHOXYBENZONITRILE
AKOS 91422
AKOS B005792
O-CYANOANISOLE
O-METHOXYBENZONITRILE
1-Cyano-2-methoxybenzene
Benzonitrile, 2-methoxy-
o-Anisonitrile
2-Methoxybenzonitrile o-Methoxybenzonitrile
2-methoxybnezonitrile
Methyl 2-cyanophenyl ether
[EINECS(EC#)]

229-559-0
[Molecular Formula]

C8H7NO
[MDL Number]

MFCD00001783
[Molecular Weight]

133.15
[MOL File]

6609-56-9.mol
Chemical PropertiesBack Directory
[Melting point ]

24.5°C
[Boiling point ]

135 °C12 mm Hg(lit.)
[density ]

1.093 g/mL at 25 °C(lit.)
[refractive index ]

n20/D 1.5465(lit.)
[Fp ]

>230 °F
[storage temp. ]

Sealed in dry,Room Temperature
[Water Solubility ]

Slightly soluble in water
[form ]

Liquid
[color ]

Clear colorless to pale yellow
[BRN ]

2207134
[InChI]

InChI=1S/C8H7NO/c1-10-8-5-3-2-4-7(8)6-9/h2-5H,1H3
[InChIKey]

FSTPMFASNVISBU-UHFFFAOYSA-N
[SMILES]

C(#N)C1=CC=CC=C1OC
[CAS DataBase Reference]

6609-56-9(CAS DataBase Reference)
[NIST Chemistry Reference]

o-Methoxybenzonitrile(6609-56-9)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S37/39:Wear suitable gloves and eye/face protection .
[RIDADR ]

3276
[WGK Germany ]

3
[HazardClass ]

6.1
[PackingGroup ]

III
[HS Code ]

29269090
Raw materials And Preparation ProductsBack Directory
[Raw materials]

o-Anisidine
[Preparation Products]

2-METHOXY-6-(5,5-DIMETHYL-1,3,2-DIOXABORINAN-2-YL)BENZONITRILE-->2-METHOXY-BENZAMIDINE HCL-->2-METHOXY-BENZAMIDINE HCL-->N'-HYDROXY-2-METHOXYBENZENECARBOXIMIDAMIDE
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

2-Methoxybenzonitrile(6609-56-9).msds
Hazard InformationBack Directory
[Chemical Properties]

Colorless liquid
[Uses]

2-Methoxybenzonitrile was used in the synthesis of 5-(4′-methyl [1,1′-biphenyl]-2-yl)-1H-tetrazole.
[Preparation]

o-Anisidine with sodium nitrite to make a diazonium salt solution, add it to the lead cyanide solution, and then add benzene. Put the mixture for 10-15h and carry out steam distillation, separate the benzene layer from the distillate, dry it with calcium chloride, evaporate the benzene, and distill the residue under reduced pressure, collect 120-122.5°C (1.2kPa fraction) to get 2-Methoxybenzonitrile, yield 64.5-67.3%.
[Synthesis Reference(s)]

Journal of the American Chemical Society, 77, p. 109, 1955 DOI: 10.1021/ja01606a035
Synthesis, p. 641, 1992
Tetrahedron Letters, 32, p. 1007, 1991 DOI: 10.1016/S0040-4039(00)74473-X
[General Description]

Surface-enhanced Raman spectra study of 2-methoxybenzonitrile has been reported.
Spectrum DetailBack Directory
[Spectrum Detail]

2-Methoxybenzonitrile(6609-56-9)MS
2-Methoxybenzonitrile(6609-56-9)1HNMR
2-Methoxybenzonitrile(6609-56-9)13CNMR
2-Methoxybenzonitrile(6609-56-9)IR1
2-Methoxybenzonitrile(6609-56-9)Raman
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

2-Methoxybenzonitrile, 98%(6609-56-9)
[Sigma Aldrich]

6609-56-9(sigmaaldrich)
[TCI AMERICA]

2-Methoxybenzonitrile,>95.0%(GC)(6609-56-9)
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