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ChemicalBook--->CAS DataBase List--->29022-11-5

29022-11-5

29022-11-5 Structure

29022-11-5 Structure
IdentificationMore
[Name]

FMOC-Glycine
[CAS]

29022-11-5
[Synonyms]

9-FLUORENYLMETHOXYCARBONYL-GLYCINE
F-FMOC-GLYCINE
FMOC-GLY
FMOC-GLYCINE
FMOC-GLY-OH
FMOC-L-GLY
FMOC-L-GLYCINE
FMOC-L-GLY-OH
N-(9-FLUORENYLMETHOXYCARBONYL)-GLYCINE
N-9-FLUORENYLMETHYLOXYCARBONYLGLYCINE
N-9-FMOC-L-GLYCINE
N-[(9H-FLUOREN-9-YLMETHOXY)CARBONYL]GLYCINE
N-ALPHA-(9-FLUORENYLMETHOXYCARBONYL)-GLYCINE
N-ALPHA-(9-FLUORENYLMETHYLOXYCARBONYL)-GLYCINE
N-ALPHA-FMOC-GLYCINE
N-FMOC-GLYCINE
N-FMOC-L-GLYCINE
npc14692
Glycine-1-13C-N-FMOC
Glycine-2-13C-N-FMOC
[EINECS(EC#)]

249-373-3
[Molecular Formula]

C17H15NO4
[MDL Number]

MFCD00037140
[Molecular Weight]

297.31
[MOL File]

29022-11-5.mol
Chemical PropertiesBack Directory
[Appearance]

white to light yellow crystal powde
[Melting point ]

174-175 °C(lit.)
[Boiling point ]

438.82°C (rough estimate)
[density ]

1.1671 (rough estimate)
[refractive index ]

1.4500 (estimate)
[storage temp. ]

2-8°C
[solubility ]

almost transparency in Methanol
[form ]

Powder
[pka]

3.89±0.10(Predicted)
[color ]

White
[Detection Methods]

HPLC,NMR
[BRN ]

2163967
[InChI]

InChI=1S/C17H15NO4/c19-16(20)9-18-17(21)22-10-15-13-7-3-1-5-11(13)12-6-2-4-8-14(12)15/h1-8,15H,9-10H2,(H,18,21)(H,19,20)
[InChIKey]

NDKDFTQNXLHCGO-UHFFFAOYSA-N
[SMILES]

C(O)(=O)CNC(OCC1C2=C(C=CC=C2)C2=C1C=CC=C2)=O
[CAS DataBase Reference]

29022-11-5(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S24/25:Avoid contact with skin and eyes .
S36:Wear suitable protective clothing .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
[WGK Germany ]

3
[HS Code ]

29242995
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

Fmoc-Gly-OH(29022-11-5).msds
Hazard InformationBack Directory
[Chemical Properties]

white to light yellow crystal powde
[Uses]

N-Fmoc-glycine is an N-Fmoc-protected form of Glycine (G615990). Glycine is a nonessential amino acid that acts as an inhibitory neyrotransmitter in the vertebrate central nervous system. Glycine also posesses cytoprotective against oxidant damage in the kidney.
[Preparation]

Glycine (Gly) (0.5 g, 6.66 mmol) was dissolved in 10% NaCO3 (14 ml) under stirring in a 50-ml flask. To the resulting solution, which had been put into an ice bath, 9-fluorenylmethoxycarbonyl chloride (Fmoc-Cl) (1.72 g, 6.66 mmol) in dioxane (12 ml) was gradually added. The reaction mixture was stirred at room temperature for 4 hours. Then added water (150 ml) to the mixture. The aqueous phase layer was separated from the reaction mixture and stripped with ether three times (75 ml×3). The stripped aqueous layer was acidified with 2N HCl aqueous solution to a pH=2, followed by extraction with ethyl acetate three times (75 ml×3). The organic phase layer was recovered and concentrated to obtain crude product of 1.70 g. The crude product was recrystallized in a mixed solvent of ethyl acetate hexane=1:2 (30 ml), and white solid denoted as Fmoc-Gly-OH was obtained after filtration at a reduced pressure.
Fmoc-Gly-OH
[General Description]

The product number for this product was previously 04-12-1001.

To obtain a certificate of analysis (CoA) of a lot that begins with the letter “A”, please select the option in the right hand menu “Request a COA for Lot#s starting with A”.
[reaction suitability]

reaction type: Fmoc solid-phase peptide synthesis
Spectrum DetailBack Directory
[Spectrum Detail]

FMOC-Glycine(29022-11-5)MS
FMOC-Glycine(29022-11-5)1HNMR
FMOC-Glycine(29022-11-5)13CNMR
FMOC-Glycine(29022-11-5)IR1
FMOC-Glycine(29022-11-5)IR2
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

FMOC-Glycine, 98%(29022-11-5)
[Alfa Aesar]

N-Fmoc-glycine, 98%(29022-11-5)
[Sigma Aldrich]

29022-11-5(sigmaaldrich)
[TCI AMERICA]

N-[(9H-Fluoren-9-ylmethoxy)carbonyl]glycine,>98.0%(LC)(T)(29022-11-5)
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