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ChemicalBook--->CAS DataBase List--->20717-86-6

20717-86-6

20717-86-6 Structure

20717-86-6 Structure
IdentificationMore
[Name]

CHLOROTITANIUM TRIISOPROPOXIDE
[CAS]

20717-86-6
[Synonyms]

CHLOROTIISOPROPOXYTITANIUM
CHLOROTITANIUM(IV) TRIISOPROPOXIDE
CHLOROTITANIUM TRIISOPROPOXIDE
CHLOROTITANIUM TRIISOPROPYLATE
CHLOROTRIISOPROPOXYTITANIUM
CHLOROTRIISOPROPYL ORTHOTITANATE
CHLOROTRIISOPROPYLOXYTITANE
CTT
ORTHOTITANIC ACID TRIISOPROPYL ESTER CHLORIDE
TITANIC ACID TRIISOPROPYL ESTER CHLORIDE
TITANIUM CHLORIDE TRIISOPROPOXIDE
TITANIUM(IV) TRIISOPROPOXY CHLORIDE
Chlorotitanium tri-i-propoxide,
CHLOROTITANIUM TRIISOPROPOXIDE, 1.0M SOL UTION IN HEXANES
Chlorotriisopropoxytitanium(IV), 95%
Titanium Chloride Triisopropoxide, 1.25M in tetrahydrofuran
CHLOROTRIISOPROPYL ORTHOTITANATE (SOLUTION 1 MOL/L IN N-HEXANE)
Chlorotitanium triisopropoxide, 1.0 M solution in dichloromethane
Chlorotitaniumtriisopropoxide,97%
Titanium, chlorotris(2-propanolato)-, (T-4)-
[EINECS(EC#)]

679-414-4
[Molecular Formula]

C9H21ClO3Ti
[MDL Number]

MFCD00009861
[Molecular Weight]

260.58
[MOL File]

20717-86-6.mol
Chemical PropertiesBack Directory
[Appearance]

Colorless to yellow liquid or low melting solid,
[Melting point ]

35-40 °C
[Boiling point ]

63-66°C 0,1mm
[density ]

1.091 g/mL at 25 °C(lit.)
[Fp ]

72 °F
[storage temp. ]

Flammables area
[solubility ]

sol most nonprotic organic solvents, e.g. Et2O, THF, CH2Cl2, toluene, hexanes
[form ]

liquid
[color ]

fused solid to pale yellow
[Specific Gravity]

1.091
[Hydrolytic Sensitivity]

7: reacts slowly with moisture/water
[Sensitive ]

Moisture Sensitive
[BRN ]

4163222
[CAS DataBase Reference]

20717-86-6(CAS DataBase Reference)
[EPA Substance Registry System]

Titanium, chlorotris(2-propanolato)-, (T-4)- (20717-86-6)
Safety DataBack Directory
[Hazard Codes ]

C,F
[Risk Statements ]

R10:Flammable.
R34:Causes burns.
R23/24/25:Toxic by inhalation, in contact with skin and if swallowed .
R11:Highly Flammable.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S27:Take off immediately all contaminated clothing .
S16:Keep away from sources of ignition-No smoking .
[RIDADR ]

UN 2924 3/PG 2
[WGK Germany ]

3
[F ]

3-10-21
[TSCA ]

No
[HazardClass ]

4.1
[PackingGroup ]

II
[HS Code ]

29051990
Hazard InformationBack Directory
[Chemical Properties]

Colorless to yellow liquid or low melting solid,
[Uses]

Chlorotriisopropoxytitanium(IV) solution may be used as a precursor for the synthesis of ultralow density ceramic materials. The product may be used to mediate a reductive amination reaction of 5α-cholestane-3,7-dione to yield aryl aminocholestanes.
[Synthesis Reference(s)]

1. Reetz, M. T.; Westermann, J.; Steinbach, R.; Wenderoth, B.; Peter, R.; Ostarek, R.; Maus, S. CB 1985, 118, 1421.
[reaction suitability]

core: titanium
reagent type: catalyst
[Synthesis]

Chlorotitanium triisopropoxide can be easily made from a 3:1 mixture of Titanium Tetraisopropoxide and Titanium(IV) Chloride,1 which can be distilled to give the pure reagent or used in situ.
[Purification Methods]

When distilled under vacuum, the distillate sets slowly to a solid on standing. Stock reagents are made by dissolving the warm liquid in pentane, toluene, Et2O, THF, CH2Cl2,, and can be stored in a pure state or in solution under dry N2 for several months. The reagent is hygroscopic and is hydrolysed by H2O. [Reetz et al. Chem Ber 118 1421 1985.]
[Precautions]

Chlorotitanium triisopropoxide is corrosive; moisture sensitive; flammable liquid; can be stored under nitrogen, in pure form or in solution, for months.
Spectrum DetailBack Directory
[Spectrum Detail]

CHLOROTITANIUM TRIISOPROPOXIDE(20717-86-6)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

Chlorotitanium triisopropoxide, 98%(20717-86-6)
[Alfa Aesar]

Chlorotitanium triisopropoxide, 95%(20717-86-6)
[Sigma Aldrich]

20717-86-6(sigmaaldrich)
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