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ChemicalBook--->CAS DataBase List--->16357-59-8

16357-59-8

16357-59-8 Structure

16357-59-8 Structure
IdentificationMore
[Name]

N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline
[CAS]

16357-59-8
[Synonyms]

1-ETHOXYCARBONYL-2-ETHOXY-1,2-DIHYDROQUINOLINE
2-ETHOXY-1,2-DIHYDRO-1-QUINOLINECARBOXYLIC ACID ETHYL ESTER
2-ETHOXY-1(2H)-QUINOLINECARBOXYLIC ACID ETHYL ESTER
2-ETHOXY-1-ETHOXYCARBONYL-1,2-DIHYDROQUINOLINE
EEDQ
ETHYL 1,2-DIHYDRO-2-ETHOXY-1-QUINOLINECARBOXYLATE
ETHYL 1,2-DIHYDRO-2-ETHOXYQUINOLINE-1-CARBOXYLATE
ETHYL 2-ETHOXY-1,2-DIHYDRO-1-QUINOLINECARBOXYLATE
LABOTEST-BB LT00440890
N-ETHOXYCARBONYL-2-ETHOXY-1,2-DIHYDROQUINOLINE
2-ethoxy-1(2h)-quinolinecarboxylicaciethylester
EEDQ~N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline
ethyl N-(2-ethoxy-1,2-dihydroquinoline)carboxylate
EEDQ (1-ETHOXY-CARBONYL-2-ETHOXY-1,2
EEDQ, 99+%, (2-ETHOXY-1-ETHOXYCARBONYL-1 ,2-DIHYDROQUINOLINE)
N-ETHOXYCARBONYL-2-ETHOXY-1,2-DIHYDROQUINOLINE 99% ( EEDQ)
Eedq(2-Ethoxy-1-Ethoxycarbonyl-1,2-Dihydroquinoline)
1,2-Dihydro-2-ethoxy-1-quinolinecarboxylicacidester
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline, 99+%
1(2H)-Quinolinecarboxylic acid, 2-ethoxy-, ethyl ester
[EINECS(EC#)]

240-418-2
[Molecular Formula]

C14H17NO3
[MDL Number]

MFCD00006703
[Molecular Weight]

247.29
[MOL File]

16357-59-8.mol
Chemical PropertiesBack Directory
[Appearance]

White to pale yellow solid
[Melting point ]

62-67 °C(lit.)
[Boiling point ]

125-128 °C (0.1 mmHg)
[density ]

1.1173 (rough estimate)
[refractive index ]

1.5300 (estimate)
[Fp ]

125-128°C/0.1mm
[storage temp. ]

2-8°C
[solubility ]

Chlorofrom (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
[form ]

Crystalline Powder
[pka]

-1.27±0.40(Predicted)
[color ]

White to beige
[Water Solubility ]

insoluble
[Sensitive ]

Moisture Sensitive
[Detection Methods]

HPLC,T
[Merck ]

14,3518
[BRN ]

533048
[CAS DataBase Reference]

16357-59-8(CAS DataBase Reference)
[EPA Substance Registry System]

16357-59-8(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xi,Xn
[Risk Statements ]

R38:Irritating to the skin.
R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[RTECS ]

VB2010000
[F ]

9-21
[TSCA ]

Yes
[HS Code ]

29334990
[Toxicity]

mouse,LD50,intraperitoneal,32mg/kg (32mg/kg),Journal of Medicinal Chemistry. Vol. 14, Pg. 49, 1971.
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Diethyl ether-->Dichloromethane-->N,N-Dimethylformamide-->Magnesium sulfate-->Potassium hydroxide-->Ethyl chloroformate-->Quinoline-->Boron trifluoride diethyl etherate
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8).msds
Hazard InformationBack Directory
[Chemical Properties]

White to pale yellow solid
[Uses]

2-Ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline is an irreversible membrane-bound receptor antagonist. It is used in synthetic chemistry, discovery, process R&D. It also acts as coupling reagents.
[Uses]

In the synthesis of peptides.
[Uses]

Peptide condensing agent with little or no racemization. Amidation coupling reagent.
[reaction suitability]

reaction type: Coupling Reactions
[Purification Methods]

Dissolve EEDQ ~180g in CHCl3, evaporate to dryness in a vacuum. Add dry Et2O (20mL) and a white solid separates on standing. Set aside for a few hours, collect the solid, wash it thoroughly with cold Et2O and dry it in a vacuum (~140g, m 63.5-65o). A further crop of solid (~25g) is obtained from the filtrate on standing overnight. [Fieser & Fieser Reagents for Organic Synthesis 2 191 1969, Belleau et al. J Am Chem Soc 90 823 1968 and 90 1651 1968, Beilstein 21/3 V 28.]
Spectrum DetailBack Directory
[Spectrum Detail]

N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)MS
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)1HNMR
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)13CNMR
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)IR1
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)IR2
N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline(16357-59-8)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline, 99+%(16357-59-8)
[Alfa Aesar]

2-Ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline, 99%(16357-59-8)
[Sigma Aldrich]

16357-59-8(sigmaaldrich)
[TCI AMERICA]

1-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline,>98.0%(T)(16357-59-8)
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