Identification | Back Directory | [Name]
CYCLODECANONE | [CAS]
1502-06-3 | [Synonyms]
NSC 90293 CYCLODECANONE Ketocyclodecane CYCLODECAN-1-ONE Cyclodecanone,97% Cyclodecanone 97% CYCLODECANONE CRYSTALLINE N-(6-amino-1-methyl-2,4-dioxo-5-pyrimidinyl)formamide | [EINECS(EC#)]
216-119-8 | [Molecular Formula]
C10H18O | [MDL Number]
MFCD00003713 | [MOL File]
1502-06-3.mol | [Molecular Weight]
154.25 |
Chemical Properties | Back Directory | [Melting point ]
21-24 °C(lit.)
| [Boiling point ]
106-107 °C12 mm Hg(lit.)
| [density ]
0.958 g/mL at 25 °C(lit.)
| [refractive index ]
n20/D 1.482(lit.)
| [Fp ]
180 °F
| [storage temp. ]
2-8°C | [solubility ]
Chloroform (Slightly), Methanol (Slightly) | [form ]
Colourless Oil to Semi-Solid | [BRN ]
1617127 | [LogP]
2.929 (est) |
Hazard Information | Back Directory | [Chemical Properties]
White solid or colorless liquid | [Synthesis Reference(s)]
Journal of the American Chemical Society, 86, p. 3068, 1964 DOI: 10.1021/ja01069a019 Organic Syntheses, Coll. Vol. 4, p. 218, 1963 Synthetic Communications, 9, p. 437, 1979 DOI: 10.1080/00397917908064174 | [Purification Methods]
Purify the ketone via the semicarbazone (m 205-207o, from EtOH) and distil it through an efficient column. It sublimes in a vacuum. The oxime has m 80o, from MeOH or by sublimation in a high vacuum. [Cope et al. Org Synth Coll Vol IV 218 1963, Prelog et al. Helv Chim Acta 30 1746 1947, Ruzicka et al. Helv Chim Acta 11 675 1930, Beilstein 7 III 134, 7 IV 76.] |
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Company Name: |
Energy Chemical
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021-021-58432009 400-005-6266 |
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http://www.energy-chemical.com |
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