TRIMETHYLSILYL TRIFLUOROACETATE synthesis
- Product Name:TRIMETHYLSILYL TRIFLUOROACETATE
- CAS Number:400-53-3
- Molecular formula:C5H9F3O2Si
- Molecular Weight:186.2
Yield: 94%
Reaction Conditions:
with CBV780 at 60; for 0.0833333 h;Microwave irradiation;
Steps:
14 Examples 2 to 85 and Comparative Examples 1and 2
The same procedure as in Example 1 was repeated with varying reaction conditions (such as catalysts, starting materials, reaction temperature, reaction time and the like), to carry out reactions, and the analyses of the resulting products. The results of the yields of the respective products as measured by gas chromatography or nuclear magnetic resonance spectroscopy are shown in Table 1-ito Table 1-7.
References:
NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY;Yamashita, Hiroshi;Hatori, Makiko;Yoshinaga, Michiyo;Han, Li-BIAO;Shimada, Shigeru;Sato, Kazuhiko US2018/44359, 2018, A1 Location in patent:Paragraph 0131
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