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ChemicalBook CAS DataBase List TERT-BUTYL 3,4,5-TRIMETHYL-2-PYRROLECARBOXYLATE
50634-31-6

TERT-BUTYL 3,4,5-TRIMETHYL-2-PYRROLECARBOXYLATE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: toluene-4-sulfonic acid / benzene; ethylene glycol / 18 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.25 h / 0 - 23 °C / Inert atmosphere
2.2: 24 h / 0 - 23 °C / Inert atmosphere
3.1: borane-THF / tetrahydrofuran / 0 - 23 °C / Inert atmosphere

References:

Beh, Michael H.R.;Figliola, Carlotta;Lund, Kate-Lyn A.R.;Kajetanowicz, Aleksandra K.;Johnsen, Ann E.;Aronitz, Elise M.;Thompson, Alison [Canadian Journal of Chemistry,2018,vol. 96,# 7,p. 779 - 784]