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ChemicalBook CAS DataBase List SPIRO[2.5]OCT-6-YL-METHANOL
849671-56-3

SPIRO[2.5]OCT-6-YL-METHANOL synthesis

3synthesis methods
-

Yield:849671-56-3 34%

Reaction Conditions:

with diethylzinc in toluene at 20 - 60; for 20 h;Simmons-Smith reaction;

References:

Irie, Osamu;Yokokawa, Fumiaki;Ehara, Takeru;Iwasaki, Atsuko;Iwaki, Yuki;Hitomi, Yuko;Konishi, Kazuhide;Kishida, Masashi;Toyao, Atsushi;Masuya, Keiichi;Gunji, Hiroki;Sakaki, Junichi;Iwasaki, Genji;Hirao, Hajime;Kanazawa, Takanori;Tanabe, Keiko;Kosaka, Takatoshi;Hart, Terance W.;Hallett, Allan [Bioorganic and Medicinal Chemistry Letters,2008,vol. 18,# 16,p. 4642 - 4646] Location in patent:scheme or table

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