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ChemicalBook CAS DataBase List Pentamethylcyclopentadienyltitanium trichloride
12129-06-5

Pentamethylcyclopentadienyltitanium trichloride synthesis

4synthesis methods
-

Yield:12129-06-5 99%

Reaction Conditions:

in toluene;Dropwise addn. of TiCl4 in toluene to soln. of C(CH3)5Si(CH3)3 in toluene (N2), stirring (2 h, color change from red-orange to red).; Evapn. of solvent and byproduct (vacuum), washing of crystals (pentane), dried (vacuum), elem. anal.;

References:

Llinas, Gerardo Hidalgo;Mena, Miguel;Palacios, Federico;Royo, Pascual;Serrano, Ricardo [Journal of Organometallic Chemistry,1988,vol. 340,p. 37 - 40]

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