N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE synthesis
- Product Name:N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE
- CAS Number:97051-69-9
- Molecular formula:C9H9F3N2O
- Molecular Weight:218.18
![Acetamide, N-[2-nitro-4-(trifluoromethyl)phenyl]-](/CAS/GIF/396-12-3.gif)
396-12-3
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97051-69-9
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Yield:-
Reaction Conditions:
with palladium on activated charcoal;hydrogen in methanol at 20; under 2585.81 Torr; for 0.333333 h;
Steps:
33.2
Step 2. The crude product from the previous step was dissolved in MeOH (20 mL) and Pd/C (catalytic) was added. The reaction mixture was shaken at room temperature under hydrogen (50 psi) for 20 minutes, then filtered through Celite. The product was concentrated and made into the azeotrope using toluene to provide crude N-(2-amino-4- (trifluoromethyl)phenyl) acetamide.
References:
WO2015/76800,2015,A1 Location in patent:Page/Page column 208
400-98-6
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97051-69-9
25 suppliers
$28.60/50mg