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ChemicalBook CAS DataBase List N,N-Dimethyloctylamine
7378-99-6

N,N-Dimethyloctylamine synthesis

13synthesis methods
-

Yield:7378-99-6 99%

Reaction Conditions:

with 5percent silver supported on titanium oxide at 25; for 6 h;Inert atmosphere;UV-irradiation;Sealed tube;

Steps:

33 Example 26
General procedure: In a glass reaction vessel, 2 mmol of benzylamine,45 mg of catalyst D,20 mL of dehydrated methanol,And a magnetic stirrer.Then, an argon gas is introduced into the sealed reaction system,Under the condition of 25 ° C.,While stirring the reaction system, ultraviolet rays were irradiated for 10 hours.Analysis of the reaction liquid showed that as a reaction product,Only N, N-dimethylbenzylamine was obtained(Yield 99% or more, see Table 5).

References:

NAGOYA UNIVERSITY;NOYORI, RYOJI;SAITO, SUSUMU;NAKA, HIROSHI;TSAREV, VASILY NIKOLAEVICH;CANER, CASADEMONT JOAQUIM JP2015/74642, 2015, A Location in patent:Paragraph 0080; 0088; 0095

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