N,N-Dibenzyl-p-anisidine synthesis
14synthesis methods
- Product Name:N,N-Dibenzyl-p-anisidine
- CAS Number:18613-55-3
- Molecular formula:C21H21NO
- Molecular Weight:303.4
Yield:18613-55-3 96%
Reaction Conditions:
Stage #1: 2,4,6-tris(4-methoxyphenyl)boroxinewith potassium carbonate in 1,4-dioxane at 130; for 24 h;Inert atmosphere;
Stage #2: N,N-dibenzyl-O-benzoylhydroxylamine in 1,4-dioxane;Inert atmosphere;
References:
Xiao, Qing;Tian, Leiming;Tan, Renchang;Xia, Ying;Qiu, Di;Zhang, Yan;Wang, Jianbo [Organic Letters,2012,vol. 14,# 16,p. 4230 - 4233] Location in patent:experimental part
