N-(MORPHOLIN-2-YLMETHYL)ACETAMIDE synthesis
- Product Name:N-(MORPHOLIN-2-YLMETHYL)ACETAMIDE
- CAS Number:112913-95-8
- Molecular formula:C7H14N2O2
- Molecular Weight:158.2
![Acetamide, N-[[4-(phenylmethyl)-2-morpholinyl]methyl]-](/CAS/20210305/GIF/112913-96-9.gif)
112913-96-9
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112913-95-8
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Yield:112913-95-8 100%
Reaction Conditions:
palladium-carbon in ethyl acetate;
Steps:
P.5.f f
f 2-(N-Acetylaminomethyl)morpholine STR27 In a solution of 2-(N-acetylaminomethyl)-4-benzylmorpholine (20 g, 80.7 mmol) in ethanol-acetic acid (20/1, 210 ml) was suspended 2.0 g of 10% palladium-carbon and the mixture was stirred at 60° C. under hydrogen stream for 22 hours. The reaction mixture was filtered with Celite, the solvent was distilled off from the filtrate under reduced pressure to give crude 2-(N-acetylaminomethyl)morpholine (15.62 g). Yield=100%. This compound was used for the subsequent reaction without purification.
References:
US5736550,1998,A
40987-25-5
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112913-95-8
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110859-48-8
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112913-95-8
19 suppliers
$155.00/100mg