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64374-53-4

N-(2,5-DIMETHYLPHENYL)HYDRAZINECARBOTHIOAMIDE synthesis

6synthesis methods
Carbamodithioic acid, (2,5-dimethylphenyl)-, monoammonium salt (9CI)

108654-39-3
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Yield:-

Reaction Conditions:

Stage #1: C9H11NS2*H3Nwith sodium monochloroacetic acid in ethanol at 20; for 0.5 h;
Stage #2: with hydrazine hydrate in ethanol at 20; for 1 h;

References:

Liu, Yang;Cui, Kunqiang;Lu, Weiqiang;Luo, Wei;Wang, Jian;Huang, Jin;Guo, Chun [Molecules,2011,vol. 16,# 6,p. 4527 - 4538] Location in patent:experimental part

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