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ChemicalBook CAS DataBase List METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE
550998-53-3

METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
1.2: 1.17 h / -78 - 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C
2.2: 1.25 h / 0 - 20 °C

References:

KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY;LEE, BYUNG HO;YI, KYU YANG;OH, KWANG SEOK;IM, CHAE JO;KIM, NAK JEONG;SO, JEE HEE;LEE, JEONG HYUN;SEO, HO WON KR2015/117318, 2015, A

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