Methyl 3-methyl-5-(trifluoromethyl)benzoate synthesis
- Product Name:Methyl 3-methyl-5-(trifluoromethyl)benzoate
- CAS Number:161622-18-0
- Molecular formula:C10H9F3O2
- Molecular Weight:218.17
99-36-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: (1,5-cyclooctadiene)(methoxy)iridium(l) dimer; 4,4'-ditert-butyl-2,2'-bipyridine / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere
2: potassium fluoride / N,N-dimethyl-formamide / 18 h / 50 °C / Inert atmosphere
References:
Litvinas, Nichole D.;Fier, Patrick S.;Hartwig, John F. [Angewandte Chemie - International Edition,2012,vol. 51,# 2,p. 536 - 539]