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    ChemicalBook CAS DataBase List METHYL 3-(4-METHYLPHENYL)-3-OXOPROPANOATE
    22027-51-6

    METHYL 3-(4-METHYLPHENYL)-3-OXOPROPANOATE synthesis

    7synthesis methods
    -

    Yield:22027-51-6 96%

    Reaction Conditions:

    Stage #1: carbonic acid dimethyl esterwith sodium hydride at 20;Inert atmosphere;
    Stage #2: para-methylacetophenone for 4 h;Inert atmosphere;Reflux;

    References:

    Balamurugan, Rengarajan;Manojveer, Seetharaman [Chemical Communications,2011,vol. 47,# 39,p. 11143 - 11145] Location in patent:supporting information; experimental part

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