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ChemicalBook CAS DataBase List MCPB
94-81-5

MCPB synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium carbonate; sodium iodide / 48 h / Reflux; Inert atmosphere
2: diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; nickel(II) bromide dimethoxyethane; 2.9-dimethyl-1,10-phenanthroline; C60H36N2 / N,N-dimethyl-formamide / 24 h / 20 °C / Molecular sieve; Irradiation

References:

Meng, Qing-Yuan;Wang, Shun;K?nig, Burkhard [Angewandte Chemie - International Edition,2017,vol. 56,# 43,p. 13426 - 13430][Angew. Chem.,2017,vol. 129,p. 13611 - 13615,5]

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