L-4'-TETRAHYDROPYRANYLGLYCINE synthesis
- Product Name:L-4'-TETRAHYDROPYRANYLGLYCINE
- CAS Number:811842-25-8
- Molecular formula:C7H13NO3
- Molecular Weight:159.18
5337-03-1
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$10.00/1 g
811842-25-8
73 suppliers
$62.00/50 mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / -10 - 0 °C
1.2: 2 h / Reflux
1.3: 1 h / -30 - 20 °C
2.1: water; potassium hydroxide; dipotassium hydrogenphosphate / methanol / 1 h / 20 °C
3.1: sodium methylate / isopropyl alcohol / 0.08 h / Cooling with ice
4.1: formate dehydrogenase; nicotinamide adenine dinucleotide; ammonia; ammonium formate; leucine dehydrogenase / water / 30 °C / pH 8-8.5 / Enzymatic reaction
References:
ASYMCHEM LABORATORIES (TIANJIN) CO., LTD;ASYMCHEM LIFE SCIENCE (TIANJIN) CO., LTD;TIANJIN ASYMCHEM PHARMACEUTICAL CO., LTD;ASYMCHEM LABORATORIES (FUXIN) CO., LTD;JILIN ASYMCHEM LABORATORIES CO., LTD.;Hong, Hao;Zheng, Changsheng;Guo, Lina US2016/319312, 2016, A1
861160-58-9
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inquiry
811842-25-8
73 suppliers
$62.00/50 mg
871261-02-8
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inquiry
811842-25-8
73 suppliers
$62.00/50 mg