Inositol synthesis
- Product Name:Inositol
- CAS Number:87-89-8
- Molecular formula:C6H12O6
- Molecular Weight:180.16
53008-65-4
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: N,N-dicyclohexylcarbodiimide; trifluoroacetic acid; pyridine / dimethylsulfoxide; benzene / 24 h / 20 °C
2: Et3N; 4-(dimethylamino)pyridine / 1,2-dichloro-ethane / 3 h / Heating
3: PdCl2 / dioxane; H2O / 3 h / 60 °C
4: NaBH4 / methanol / 0.5 h / 0 °C
5: NaOH / methanol / 12 h / 20 °C
6: 18.2 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C
References:
Takahashi;Kittaka;Ikegami [Journal of Organic Chemistry,2001,vol. 66,# 8,p. 2705 - 2716]
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![[(2S,3R,5S,6S)-2,3,4,5,6-pentahydroxycyclohexyl]oxyphosphonic acid](/CAS/GIF/15421-51-9.gif)
15421-51-9
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87-89-8
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