IFLAB-BB F2108-0089 synthesis
- Product Name:IFLAB-BB F2108-0089
- CAS Number:284462-78-8
- Molecular formula:C13H13N3O2
- Molecular Weight:243.26
827029-02-7
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Yield:284462-78-8 92%
Reaction Conditions:
with hydrogen;nickel in tetrahydrofuran;methanol at 20;
Steps:
1
The thus obtained product is hydrogenated at room temperature using Raney-nickel in MEOH/THF. The reaction solution is filtered through A Seitz-filter, rinsed with MEOH and the filtrate is subsequently evaporated. The residue is taken up in DICHLOROMETHANE, dried over Na2SO4, filtered and evaporated. Yield : 2. 29 g (92 %) 5G, brown oil
References:
WO2005/4863,2005,A1 Location in patent:Page/Page column 132
591-27-5
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98-98-6
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24484-93-3
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