ETHYLALUMINUM DICHLORIDE synthesis
- Product Name:ETHYLALUMINUM DICHLORIDE
- CAS Number:563-43-9
- Molecular formula:C2H5AlCl2
- Molecular Weight:126.95
7446-70-0
700 suppliers
$15.00/25g
100-99-2
109 suppliers
$81.09/100ml
563-43-9
78 suppliers
$12.19/10ml
1779-25-5
74 suppliers
$45.00/10g
Yield:-
Reaction Conditions:
in diethyl ether;tolueneall manipulations under dry, O2 free N2 atm.; AlCl3 dissolved in Et2O, soln. of iso-Bu3Al in toluene added at -78°C, allowed to warm to room temp., stirred and refluxed for for 3, stirred at room temp. for 48 h h;
References:
Schumann, Herbert;Dechert, Sebastian;Hummert, Markus;Lange, Katharina C. H.;Schutte, Stefan;Wassermann, Birgit C.;Koehler, Katrin;Eichhorn, Jens [Zeitschrift fur Anorganische und Allgemeine Chemie,2004,vol. 630,# 8-9,p. 1196 - 1204]
75-00-3
221 suppliers
$29.39/crm40015
563-43-9
78 suppliers
$12.19/10ml
7647-01-0
11 suppliers
$10.00/10g
96-10-6
119 suppliers
$60.50/100g
563-43-9
78 suppliers
$12.19/10ml
97-93-8
153 suppliers
$27.50/10 x 3 pellets
76-83-5
709 suppliers
$6.00/25g
563-43-9
78 suppliers
$12.19/10ml