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ChemicalBook CAS DataBase List ETHYL 2-METHYLBENZOYLFORMATE
66644-67-5

ETHYL 2-METHYLBENZOYLFORMATE synthesis

11synthesis methods
-

Yield:66644-67-5 91%

Reaction Conditions:

Stage #1: 2-methylchlorobenzenewith lithium in diethyl ether at 3 - 6;
Stage #2: with copper(l) cyanide in tetrahydrofuran;diethyl ether at 3 - 6; for 0.416667 h;Cooling with ice;
Stage #3: Ethyl oxalyl chloride in tetrahydrofuran;diethyl ether at 3 - 20; for 1.25 h;

References:

Screttas, Constantinos G.;Steele, Barry R.;Micha-Screttas, Maria;Heropoulos, Georgios A. [Organic Letters,2012,vol. 14,# 22,p. 5680 - 5683] Location in patent:supporting information

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