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ChemicalBook CAS DataBase List Ethanone,1-(2-amino-5-bromo-4-chlorophenyl)-
937816-91-6

Ethanone,1-(2-amino-5-bromo-4-chlorophenyl)- synthesis

2synthesis methods
21402-26-6 Synthesis
4-BROMO-3-CHLOROANILINE

21402-26-6
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Ethanone,1-(2-amino-5-bromo-4-chlorophenyl)-

937816-91-6
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Yield:-

Reaction Conditions:

Stage #1: 4-bromo-3-chloroaniline;acetonitrilewith boron trichloride in n-heptane;
Stage #2: with aluminium trichloride in n-heptane;Heating;
Stage #3: with hydrogenchloride in n-heptane;Heating;Further stages.;

References:

Nittoli, Thomas;Curran, Kevin;Insaf, Shabana;DiGrandi, Martin;Orlowski, Mark;Chopra, Rajiv;Agarwal, Atul;Howe, Anita Y. M.;Prashad, Amar;Floyd, M. Brawner;Johnson, Bernard;Sutherland, Alan;Wheless, Karen;Feld, Boris;O'Connell, John;Mansour, Tarek S.;Bloom, Jonathan [Journal of Medicinal Chemistry,2007,vol. 50,# 9,p. 2108 - 2116]

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