DIMETHYLSILYLDIETHYLAMINE synthesis

3synthesis methods

Product Name:DIMETHYLSILYLDIETHYLAMINE
CAS Number:13686-66-3
Molecular formula:C6H17NSi
Molecular Weight:131.29

by treatment of commercially available chlorodimethylsilane (ClMe2SiH) and diethylamine in the presence of triethylamine in ether, followed by filtration and distillation.

4669-59-4
112 suppliers
$41.00/5mL

13686-66-3
56 suppliers
$52.70/5g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 80 percent / Me₂SiCl₂ / 6 h / 20 °C
2: 80 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

References:

Chrusciel [Canadian Journal of Chemistry,2000,vol. 78,# 11,p. 1405 - 1411]

FullText

6026-02-4
7 suppliers
inquiry

13686-66-3
56 suppliers
$52.70/5g

References

1066-35-9 Synthesis

1066-35-9
234 suppliers
$28.00/25mL

109-89-7
467 suppliers
$10.00/5g

13686-66-3
56 suppliers
$52.70/5g

References

DIMETHYLSILYLDIETHYLAMINE Related Search:

1-TRIMETHYLSILYL-2-PYRROLIDINONE N-TRIMETHYLSILYLPHTHALIMIDE 1-CYANOETHYL(DIETHYLAMINO)DIMETHYLSILANE (4S)-N-(TERT-BUTYLDIMETHYLSILYL)AZETIDIN-2-ONE-4-CARBOXYLIC ACID