CYCLOPENTADECANE synthesis
- Product Name:CYCLOPENTADECANE
- CAS Number:295-48-7
- Molecular formula:C15H30
- Molecular Weight:210.4
111-24-0
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran / 0.5 h / -60 °C
1.2: 4 h / -60 - 20 °C
2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran / 1 h / -78 °C
2.2: 11 h / -78 - 20 °C
3.1: lithium aluminium tetrahydride
4.1: triethylamine
5.1: 640 °C / 0 Torr / Pyrolysis
6.1: Raney nickel / ethanol; acetone / 1 h / 60 °C / Inert atmosphere
References:
Trahanovsky, Walter S.;Klumpp, Douglas A. [Tetrahedron Letters,2016,vol. 57,# 22,p. 2386 - 2389]
4727-18-8
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![7,8,15,16,23,24-hexaoxatrispiro[5.2.5.2.5.2]tetracosane](/CAS/GIF/182-01-4.gif)
182-01-4
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295-48-7
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