ChemicalBook CAS DataBase List cis-3-Hexenyl benzoate

cis-3-Hexenyl benzoate synthesis

5synthesis methods

Product Name:cis-3-Hexenyl benzoate
CAS Number:25152-85-6
Molecular formula:C13H16O2
Molecular Weight:204.26

Cis-3-Hexenyl benzoate is prepared by estcrification of cis-3-Hcxcnol with Bcnzoic acid (or with BcrKoyl chloride).

928-96-1 Synthesis

928-96-1
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$14.00/1g

94-36-0 Synthesis

94-36-0
485 suppliers
$20.60/1vl

25152-85-6
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$31.00/25mL

Yield:25152-85-6 70%

Reaction Conditions:

with 1H-imidazole in acetonitrile for 6 h;Reflux;

Steps:

Typical procedure for the synthesis of phenolic benzoate
General procedure: Alcohols (0.1 mL,1 mmol) was added to a stirred solution of imidazole (0.272 g, 4.0 mmol) and benzoyl peroxide (0.363 g, 1.5 mmol) in 5 mL of CH3CN at reflux. The reactionwas monitored by TLC. After completion of the reaction (3 h), the solvent wasevaporated and the residue was subjected to purification on a short column ofsilica gel, using n-hexane/EtOAc (4:1) as the eluent to give phenolic benzoate.

References:

Nowrouzi, Najmeh;Alizadeh, Seyedeh Zahra [Tetrahedron Letters,2013,vol. 54,# 19,p. 2412 - 2414]

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928-96-1 Synthesis

928-96-1
475 suppliers
$14.00/1g

98-88-4 Synthesis