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ChemicalBook CAS DataBase List Cinnamyl chloride
21087-29-6

Cinnamyl chloride synthesis

14synthesis methods
-

Yield:21087-29-6 83%

Reaction Conditions:

with FeCl2(phen)3 in acetonitrile at 60; for 0.5 h;

Steps:

General procedure B. Fe(phen)3Cl2 mediated chlorination of iodoalkanes
General procedure: To a solution of iodoalkanes (0.12 mmol, 1.0 equiv) in CH3CN (1.2 mL) was added Fe(phen)3Cl2 (0.12 mmol, 1.0 equiv). After being stirred at 60 oC for the proper reaction time, solvent evaporation and silica gel column chromatography afforded the corresponding alkyl chloride product

References:

Hwang, Joon Young;Shin, Jung Ha;Seong, Eun Young;Kang, Eun Joo [Bulletin of the Korean Chemical Society,2018,vol. 39,# 5,p. 695 - 698] Location in patent:supporting information

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