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        ChemicalBook
        CAS DataBase List
        CHLOROTRIBENZYLSILANE
        
    
      
    
      
        
      
            
      
                18740-59-5
            
      
        
      
        
      
            CHLOROTRIBENZYLSILANE synthesis
        
      
        
      10synthesis methods
      
        
    
      

    
    
      
        
      
            It is prepared by reaction of benzylmagnesium
chloride with SiCl4 in ether; separation from mono- and
dibenzylated chlorosilane byproducts is then accomplished by
fractional distillation (boiling range 300–360 °C/100 mmHg).
Other preparations involve the chlorination of tribenzylsilane
using Cl2
 or an acyl chloride. No yields are reported for any
of the above preparative procedures.
            
        
      
    
      
    
    
      
        
        
      
            
            
            
            
      
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      Yield:-
      
                
                
      Reaction Conditions:
      
                
      with tetrachloromethane;chlorine
      
                
                
      References:
      
                
      
                    Jenkins;Post [Journal of Organic Chemistry,1950,vol. 15,p. 552,554]
                
      
                
            
      
            
        
      
        
        
        
        
        
        
        
        
        
    
      

    
    
      
        
        
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